Bis(trimethoxysilylpropyl)amine

Base Information

• Chemical Name: Bis(trimethoxysilylpropyl)amine
• CAS No.: 82985-35-1
• Deprecated CAS: 154608-42-1
• Molecular Formula: C12H31NO6Si2
• Molecular Weight: 341.552
• Hs Code.: 29319090
• European Community (EC) Number: 280-084-5,403-480-3
• UNII: 6H96M8992G
• DSSTox Substance ID: DTXSID6033825
• Nikkaji Number: J278.704K
• Wikidata: Q27264921
• ChEMBL ID: CHEMBL1392440
• Mol file: 82985-35-1.mol

Synonyms:bis(trimethoxysilylpropyl)amine

Chemical Property of Bis(trimethoxysilylpropyl)amine

Chemical Property:

• Appearance/Colour: COA
• Vapor Pressure: 0.003mmHg at 25°C
• Melting Point: <0 °C
• Refractive Index: n20/D 1.432(lit.)
• Boiling Point: 316.1 °C at 760 mmHg
• PKA: 10.78±0.19(Predicted)
• Flash Point: 145 °C
• PSA: 67.41000
• Density: 0.989 g/cm³
• LogP: 1.50330
• Storage Temp.: 2-8°C(protect from light)
• Water Solubility.: 34-1000g/L at 20℃
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 7
• Rotatable Bond Count: 14
• Exact Mass: 341.16899078
• Heavy Atom Count: 21
• Complexity: 211

Purity/Quality:

99%, ^*data from raw suppliers

Bis(trimethoxysilylpropyl)amine ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xn
• Hazard Codes: Xn
• Statements: 20/22-36/37/38
• Safety Statements: 26-36/37/39

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

• Canonical SMILES: CO[Si](CCCNCCC[Si](OC)(OC)OC)(OC)OC
• Uses: BTMSPA and 1,2-bis(triethoxysilyl)ethane (BTESE) can be used to synthesize an amine modified mesostructured organosilica for potential applications in catalysis and absorbance. Metal finishing may be deviced by coating BTMSPA and vinyltriacetoxysilane which can be used for protection against corrosion. Bis(trimethoxysilylpropyl)amine is used in method for dyeing keratinous material, comprising the use of an organosilicon compound, an effect pigment and a film-forming polymer.

Technology Process of Bis(trimethoxysilylpropyl)amine

There total 5 articles about Bis(trimethoxysilylpropyl)amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

3-(trimethoxysilyl)propan-1-amine (13822-56-5) + ethylenediamine (107-15-3,85404-18-8) + 3-Chloropropyltrimethoxysilan (2530-87-2) → 3-(trimethoxysilyl)-N,N-bis[3-(trimethoxysilyl)propyl]-1-propanamine + N,N-bis-(3-trimethoxysilylpropyl)amine (82985-35-1)

Guidance literature:

3-(trimethoxysilyl)propan-1-amine; ethylenediamine; 3-Chloropropyltrimethoxysilan; at 130 ℃; for 6h;

With ethylenediamine; at 110 ℃; for 0.05h;

Reference yield: 81.0%

3-(trimethoxysilyl)propan-1-amine (13822-56-5) + 3-Chloropropyltrimethoxysilan (2530-87-2) → 2,2-dimethoxy-1-(3-trimethoxysilylpropyl)-1-aza-2-silacyclopentane (109084-60-8) + N,N-bis-(3-trimethoxysilylpropyl)amine (82985-35-1)

Guidance literature:

3-(trimethoxysilyl)propan-1-amine; 3-Chloropropyltrimethoxysilan; at 130 ℃; for 6h;

With ethylenediamine; at 110 ℃; for 1.16667h;

Reference yield:

3-(trimethoxysilyl)propan-1-amine (13822-56-5) + 3-Chloropropyltrimethoxysilan (2530-87-2) → N,N-bis-(3-trimethoxysilylpropyl)amine (82985-35-1)

Guidance literature:

With methanol; at 20 ℃; for 0.5h;

upstream raw materials:

3-(trimethoxysilyl)propan-1-amine

3-Chloropropyltrimethoxysilan

ethylenediamine

Downstream raw materials:

2-nitrobenzyl bis(trimethoxysilylpropyl)carbamate

4-{[Bis-(3-trimethoxysilanyl-propyl)-amino]-methyl}-benzaldehyde

Refernces

• 1、 -. "TWO-COMPONENT SYSTEM FOR SMOOTHING AND CARE OF HAIR". . . Retrieved 2022/01/23.
• 2、 -. "PROCESS FOR DYEING HAIR". . . Retrieved 2021/01/22.