2-METHOXY-2,4-DIPHENYL-3(2H)-FURANONE

Base Information

• Chemical Name: 2-METHOXY-2,4-DIPHENYL-3(2H)-FURANONE
• CAS No.: 50632-57-0
• Molecular Formula: C17H14 O3
• Molecular Weight: 266.296
• Hs Code.: 2932190090
• Mol file: 50632-57-0.mol

Synonyms:2-Methoxy-2,4-diphenyl-3(2H)-furanone

Chemical Property of 2-METHOXY-2,4-DIPHENYL-3(2H)-FURANONE

Chemical Property:

• Vapor Pressure: 1.75E-07mmHg at 25°C
• Melting Point: 96°C
• Boiling Point: 426.6°C at 760 mmHg
• Flash Point: 203.6°C
• PSA: 35.53000
• Density: 1.22g/cm³
• LogP: 3.12620
• Storage Temp.: 2-8°C

Purity/Quality:

98%,99%, ^*data from raw suppliers

2-Methoxy-2,4-diphenyl-3(2H)-furanone ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26-36

MSDS Files:

SDS file from LookChem

Useful:

• Uses: 2-Methoxy-2,4-diphenyl-3(2H)-furanone (cas# 50632-57-0) is a compound useful in organic synthesis. 2-Methoxy-2,4-diphenyl-3(2H)-furanone (MDPF) is used as a fluorescence reagent to derivatize primary and secondary amines on molecules such as proteins. MDPF derivatized molecules can be detected during analytical and separation procedures including chromatography, electrophoresis and zymography.

Technology Process of 2-METHOXY-2,4-DIPHENYL-3(2H)-FURANONE

There total 3 articles about 2-METHOXY-2,4-DIPHENYL-3(2H)-FURANONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

aqueous potassium hydroxide + 1-dimethylamino-2,4-diphenyl-1-butene-3,4-dione (36777-65-8) → 2-methoxy-2,4-diphenyl-3-(2H)-furanone (50632-57-0)

Guidance literature:

In methanol; ethanol; chloroform;

Reference yield:

1,3-diphenylpropane-1,2-dione (23464-17-7) → 2-methoxy-2,4-diphenyl-3-(2H)-furanone (50632-57-0)

Guidance literature:

Multi-step reaction with 2 steps

1: N,N-dimethyl-formamide dimethyl acetal; Petroleum ether

2: methanol; ethanol; chloroform

In methanol; ethanol; chloroform; N,N-dimethyl-formamide dimethyl acetal; Petroleum ether;

Reference yield:

→ 2-methoxy-2,4-diphenyl-3-(2H)-furanone (50632-57-0)

Guidance literature:

Alkohol (7), MeOH;

DOI:10.1021/jo00864a051

upstream raw materials:

1-dimethylamino-2,4-diphenyl-1-butene-3,4-dione

1,3-diphenylpropane-1,2-dione

Downstream raw materials:

(E)-4-Dimethylamino-1,3-diphenyl-but-3-ene-1,2-dione

1-ethyl-2-hydroxy-2,4-diphenyl-1,2-dihydro-pyrrol-3-one

Refernces