3-(Dibutylamino)propylamine

Base Information

• Chemical Name: 3-(Dibutylamino)propylamine
• CAS No.: 102-83-0
• Molecular Formula: C11H26N2
• Molecular Weight: 186.341
• Hs Code.: 2921290000
• European Community (EC) Number: 203-059-2
• NSC Number: 7777,6333
• UNII: 3SFY0J0731
• DSSTox Substance ID: DTXSID8059261
• Nikkaji Number: J35.158J
• Wikidata: Q27257978
• ChEMBL ID: CHEMBL534299
• Mol file: 102-83-0.mol

Synonyms:102-83-0;3-(Dibutylamino)propylamine;N,N-Dibutyl-1,3-propanediamine;N1,N1-Dibutylpropane-1,3-diamine;N,N-Dibutyltrimethylenediamine;N,N-Dibutylaminopropylamine;(3-Aminopropyl)Dibutylamine;1,3-Propanediamine, N1,N1-dibutyl-;3-(Di-n-butylamino)propylamine;3-Aminopropyldibutylamine;1,3-PROPANEDIAMINE, N,N-DIBUTYL-;N',N'-dibutylpropane-1,3-diamine;NSC 6333;N,N-Dibutyl-1,3-diaminopropane;EINECS 203-059-2;BRN 0635829;UNII-3SFY0J0731;AI3-25437;3-(Dibutylamino)-1-propylamine;3SFY0J0731;NSC-6333;NSC-7777;1, N,N-dibutyl-;4-04-00-01262 (Beilstein Handbook Reference);WLN: Z3N4 & 4;3-(Dibutylamino)-n-propylamine;NSC6333;N,N-di-n-Butyl-1,3-propanediamine;3-(di-Normal-butylamino)-propylamine;MFCD00008219;dibutylaminopropylamine;3-aminopropyldibutylamin;3-dibutylaminopropylamine;3-aminopropyl-dibutyl-amine;SCHEMBL181644;CHEMBL534299;DTXSID8059261;NSC7777;3-(Dibutylamino)propylamine, 98%;N-AMINOPROPYL-N,N-DIBUTYLAMINE;AKOS009158401;CS-W016886;LS-119799;D1078;FT-0629445;D97282;3-(N,N-DI-N-BUTYLAMINO)-1-AMINOPROPANE;EN300-8045904;J-000811;Q27257978;Z330828934

Chemical Property of 3-(Dibutylamino)propylamine

Chemical Property:

• Appearance/Colour: Clear colourless liquid
• Vapor Pressure: 0.256mmHg at 25°C
• Melting Point: -50 °C
• Refractive Index: n20/D 1.4463(lit.)
• Boiling Point: 204.999 °C at 760 mmHg
• PKA: 10.17±0.10(Predicted)
• Flash Point: 103.889 °C
• PSA: 29.26000
• Density: 0.843 g/cm³
• LogP: 2.93770
• Storage Temp.: Keep in dark place,Inert atmosphere,Room temperature
• Sensitive.: Air Sensitive
• Water Solubility.: 10 G/L (20 ºC)
• XLogP3: 2.2
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 9
• Exact Mass: 186.209598838
• Heavy Atom Count: 13
• Complexity: 86.1

Purity/Quality:

98% ^*data from raw suppliers

3-(Dibutylamino)propylamine >98.0%(GC)(T) ^*data from reagent suppliers

Safty Information:

• Pictogram(s): C
• Hazard Codes: C,Xi
• Statements: 34-36/37/38
• Safety Statements: 26-36/37/39-45-36

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

• Canonical SMILES: CCCCN(CCCC)CCCN

Technology Process of 3-(Dibutylamino)propylamine

There total 6 articles about 3-(Dibutylamino)propylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-(dibutylamino)propanenitrile (25726-99-2) → 3-dibutylaminopropylamine (102-83-0)

Guidance literature:

With ethanol; sodium;

Reference yield:

dibutylamine (111-92-2) → 3-dibutylaminopropylamine (102-83-0)

Guidance literature:

Multi-step reaction with 2 steps

2: Raney nickel; ethanol / 70 °C / 2942.03 Torr / Hydrogenation

With ethanol; nickel;

Reference yield:

2-(3-bromopropyl)isoindole-1,3-dione (5460-29-7) + dibutylamine (111-92-2) → 3-dibutylaminopropylamine (102-83-0)

Guidance literature:

With xylene; at 140 - 150 ℃; Kochen des erhaltenen N-<3-Dibutylamino-propyl>-phthalimids mit konz.HCl.;

upstream raw materials:

2-(3-bromopropyl)isoindole-1,3-dione

dibutylamine

3-(dibutylamino)propanenitrile

N-(3-dibutylamino-propyl)-phthalimide

Downstream raw materials:

2-(3-dibutylaminopropylamino)-nitrobenzene

2-{[3-(dibutylamino)propyl]amino}naphthalene-1,4-dione

Refernces

• 1、 -. "Novel monoazo and disazo colorants". . . Retrieved 2008/06/13.
• 2、 -. "Novel compositions and processes". . . Retrieved 2008/06/13.