2-Benzoyl-6-nitrobenzoic acid

Base Information

• Chemical Name: 2-Benzoyl-6-nitrobenzoic acid
• CAS No.: 7335-77-5
• Molecular Formula: C14H9NO5
• Molecular Weight: 271.229
• Mol file: 7335-77-5.mol

Synonyms:2-Benzoyl-6-nitro-benzoesaeure;2-benzoyl-6-nitro-benzoic acid;6-nitro-o-benzoylbenzoic acid;6-Nitro-o-benzoyl-benzoesaeure;Benzoic acid,2-benzoyl-6-nitro;6-Benzoyl-2-nitrobenzoesaeure;3-Nitro-benzophenon-carbonsaeure-(2);

Chemical Property of 2-Benzoyl-6-nitrobenzoic acid

Chemical Property:

• PSA: 100.19000
• LogP: 3.04720

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-Benzoyl-6-nitrobenzoic acid

There total 13 articles about 2-Benzoyl-6-nitrobenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

3-nitrophthalic acid anhydride (641-70-3) + phenylmagnesium bromide → 6-nitro-o-benzoylbenzoic acid (7335-77-5)

Guidance literature:

With N,N,N,N,-tetramethylethylenediamine; In tetrahydrofuran; at -78 ℃;

Reference yield:

2-methyl-3-nitro-benzophenone (59394-73-9) → 6-nitro-o-benzoylbenzoic acid (7335-77-5)

Guidance literature:

With hydrogenchloride; nitric acid; In water;

Reference yield:

2-methyl-3-nitrobenzic acid (1975-50-4) → 6-nitro-o-benzoylbenzoic acid (7335-77-5)

Guidance literature:

Multi-step reaction with 3 steps

1: thionyl chloride

2: hydrogenchloride; sodium carbonate / aluminium trichloride / water; benzene

3: hydrogenchloride; nitric acid / water

With hydrogenchloride; thionyl chloride; nitric acid; sodium carbonate; aluminium trichloride; In water; benzene;

upstream raw materials:

diethyl ether

3-nitrophthalic acid anhydride

diphenyl cadmium

phenylzinc(II) bromide

Downstream raw materials:

(7-Nitro-1-oxo-4-phenyl-1H-phthalazin-2-yl)-acetic acid ethyl ester

3-nitrobenzophenone

6-nitro-o-benzoylbenzoic acid chloride

1-nitroanthraquinone

Refernces

• 1、 -. "Process for preparing highly pure 1-nitroanthraquinone". . . Retrieved 2008/06/13.