Cyclohexane, propoxy-

Base Information

• Chemical Name: Cyclohexane, propoxy-
• CAS No.: 78917-92-7
• Molecular Formula: C9H18O
• Molecular Weight: 142.241
• Mol file: 78917-92-7.mol

Synonyms:n-Propyl-cyclohexyl-ether;cyclohexyl n-propyl ether;Propyloxy-cyclohexan;Cyclohexyl-propyl-aether;

Chemical Property of Cyclohexane, propoxy-

Chemical Property:

• Boiling Point: 171.2±8.0 °C(Predicted)
• PSA: 9.23000
• Density: 0.85±0.1 g/cm3(Predicted)
• LogP: 2.74570

Purity/Quality:

99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Cyclohexane, propoxy-

There total 10 articles about Cyclohexane, propoxy- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

propan-1-ol (71-23-8) + cyclohexene (110-83-8) → cyclohexyl-propyl ether (78917-92-7)

Guidance literature:

With Raney-nickel cathode; tetraethylammonium bromide; electrolysis;

DOI:10.1246/cl.1987.995

Reference yield:

propoxybenzene (622-85-5) + semicarbazide hydrochloride (563-41-7) + acetic acid (64-19-7,77671-22-8) → propan-1-ol (71-23-8) + cyclohexane (110-82-7,25012-93-5) + cyclohexyl-propyl ether (78917-92-7) + cyclohexanol (108-93-0)

Guidance literature:

Hydrogenation;

Reference yield:

3-phenoxy-2-propanone (621-87-4) → cyclohexyl-propyl ether (78917-92-7)

Guidance literature:

Multi-step reaction with 3 steps

1: LiAlH₄ / diethyl ether

2: H₂ / Rh-Al₂O₃

3: (i) SOCl₂, (ii) LiAlH₄

With lithium aluminium tetrahydride; hydrogen; rhodium on alumina; In diethyl ether;

DOI:10.1021/ja00871a020

upstream raw materials:

Cyclohexanon-di-n-propylacetal

1-cyclohexyloxy-propan-2-ol

propan-1-ol

cyclohexanone

Refernces

• 1、 Yamada, Tsukasa,Osa, Tetsuo,Matsue, Tomokazu. "Addition of Alcohol to Olefinic Bonds by Paired Electrosynthesis with Raney-Nickel Cathode". . p. 995 - 996. Retrieved 2007/10/02.