Technology Process of Methanone, (6-imino-2,4-cyclohexadien-1-ylidene)-
There total 9 articles about Methanone, (6-imino-2,4-cyclohexadien-1-ylidene)- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: pyridinium chlorochromate / dichloromethane / 15 h / 20 °C / Inert atmosphere
2: sodium azide / N,N,N,N,N,N-hexamethylphosphoric triamide / 48 h / 20 °C / Inert atmosphere
3: methyl cyclohexane / 0.67 h / -268.96 °C / UV-irradiation; Inert atmosphere
4: 14.3 h / -263.16 °C / Darkness; Inert atmosphere
With
sodium azide; pyridinium chlorochromate;
In
N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane; methyl cyclohexane;
DOI:10.1021/jacs.6b07368
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium azide / N,N,N,N,N,N-hexamethylphosphoric triamide / 48 h / 20 °C / Inert atmosphere
2: methyl cyclohexane / 0.67 h / -268.96 °C / UV-irradiation; Inert atmosphere
3: 14.3 h / -263.16 °C / Darkness; Inert atmosphere
With
sodium azide;
In
N,N,N,N,N,N-hexamethylphosphoric triamide; methyl cyclohexane;
DOI:10.1021/jacs.6b07368
- Guidance literature:
-
Multi-step reaction with 2 steps
1: methyl cyclohexane / 0.67 h / -268.96 °C / UV-irradiation; Inert atmosphere
2: 14.3 h / -263.16 °C / Darkness; Inert atmosphere
In
methyl cyclohexane;
DOI:10.1021/jacs.6b07368