4-(Pentylnitrosoamino)-1-butanol

Base Information

• Chemical Name: 4-(Pentylnitrosoamino)-1-butanol
• CAS No.: 61734-86-9
• Molecular Formula: C9H20N2O2
• Molecular Weight: 188.31
• Mol file: 61734-86-9.mol

Synonyms:N-Nitroso-N-pentyl-(4-hydroxybutyl)-amine;N-Amyl-N-(4-hydroxybutyl)nitrosamine;N-Pentyl-N-(4-hydroxybutyl)nitrosamine;4-Amyl-N-(4-hydroxybutyl)nitrosamine;1-BUTANOL,4-(PENTYLNITROSAMINO);

Chemical Property of 4-(Pentylnitrosoamino)-1-butanol

Chemical Property:

• Vapor Pressure: 9.27E-06mmHg at 25°C
• Refractive Index: 1.5800 (estimate)
• Boiling Point: 334.1°Cat760mmHg
• Flash Point: 155.8°C
• PSA: 52.90000
• Density: 1g/cm³
• LogP: 1.93250

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-(Pentylnitrosoamino)-1-butanol

There total 1 articles about 4-(Pentylnitrosoamino)-1-butanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-Chloro-1-butanol (928-51-8) + n-Pentylamine (110-58-7) → N-amyl-N-(4-hydroxybutyl)nitrosamine (61734-86-9,74778-56-6,74778-75-9)

Guidance literature:

Multistep reaction; (i), (ii) NaNO₂, aq. HCl;

DOI:10.1248/cpb.26.3891

Reference yield:

N-amyl-N-(4-hydroxybutyl)nitrosamine (61734-86-9,74778-56-6,74778-75-9) → N-amyl-N-(3-carboxypropyl)nitrosamine (62018-94-4)

Guidance literature:

With potassium hydroxide; potassium permanganate;

DOI:10.1248/cpb.26.3909

Reference yield:

N-amyl-N-(4-hydroxybutyl)nitrosamine (61734-86-9,74778-56-6,74778-75-9) → C17H23BrN2O4 (70103-68-3)

Guidance literature:

Multi-step reaction with 2 steps

1: aq. KOH, KMnO₄

2: (i) aq. NaOH, (ii) /BRN= 607604/, aq. HCl

With potassium hydroxide; potassium permanganate;

DOI:10.1248/cpb.26.3909

upstream raw materials:

4-Chloro-1-butanol

n-Pentylamine

Downstream raw materials:

N-amyl-N-(3-carboxypropyl)nitrosamine

C₁₇H₂₃BrN₂O₄

Refernces