4-[(acetyloxy)methyl]-7-methyl-1,3-dioxepane-5,6-diyl diacetate (non-preferred name)

Base Information

• Chemical Name: 4-[(acetyloxy)methyl]-7-methyl-1,3-dioxepane-5,6-diyl diacetate (non-preferred name)
• CAS No.: 7464-30-4
• Molecular Formula: C₁₃H₂₀O₈
• Molecular Weight: 304.297
• Mol file: 7464-30-4.mol

Synonyms:

Chemical Property of 4-[(acetyloxy)methyl]-7-methyl-1,3-dioxepane-5,6-diyl diacetate (non-preferred name)

Chemical Property:

• Vapor Pressure: 1.04E-05mmHg at 25°C
• Boiling Point: 371.3°Cat760mmHg
• Flash Point: 161.4°C
• Density: 1.22g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-[(acetyloxy)methyl]-7-methyl-1,3-dioxepane-5,6-diyl diacetate (non-preferred name)

There total 4 articles about 4-[(acetyloxy)methyl]-7-methyl-1,3-dioxepane-5,6-diyl diacetate (non-preferred name) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

L-rhamnitol (488-28-8) → O3,O4,O6-triacetyl-O2,O5-methanediyl-1-deoxy-L-mannitol (7464-30-4)

Guidance literature:

Multi-step reaction with 4 steps

1: aqueous hydrochloric acid

2: acetic acid; sulfuric acid

3: barium methylate; methanol

4: sodium acetate

With hydrogenchloride; methanol; sulfuric acid; sodium acetate; barium methoxide; acetic acid;

DOI:10.1021/ja01226a055

Reference yield:

O4-acetoxymethyl-O3,O6-diacetyl-O2,O5-methanediyl-1-deoxy-L-mannitol (55645-93-7) → O3,O4,O6-triacetyl-O2,O5-methanediyl-1-deoxy-L-mannitol (7464-30-4)

Guidance literature:

Multi-step reaction with 2 steps

1: barium methylate; methanol

2: sodium acetate

With methanol; sodium acetate; barium methoxide;

DOI:10.1021/ja01226a055

Reference yield:

O2,O5;O4,O6-dimethanediyl-1-deoxy-L-mannitol (55645-89-1) → O3,O4,O6-triacetyl-O2,O5-methanediyl-1-deoxy-L-mannitol (7464-30-4)

Guidance literature:

Multi-step reaction with 3 steps

1: acetic acid; sulfuric acid

2: barium methylate; methanol

3: sodium acetate

With methanol; sulfuric acid; sodium acetate; barium methoxide; acetic acid;

DOI:10.1021/ja01226a055

upstream raw materials:

acetic anhydride

O²,O⁵-methanediyl-1-deoxy-L-mannitol

L-rhamnitol

O⁴-acetoxymethyl-O³,O⁶-diacetyl-O²,O⁵-methanediyl-1-deoxy-L-mannitol