3,3'-Dichloro-N,N'-diacetylbenzidine

Base Information

• Chemical Name: 3,3'-Dichloro-N,N'-diacetylbenzidine
• CAS No.: 35958-51-1
• Molecular Formula: C₁₆H₁₄Cl₂N₂O₂
• Molecular Weight: 337.205
• Hs Code.: 2924299090
• DSSTox Substance ID: DTXSID9036858
• Nikkaji Number: J71.179I
• Wikidata: Q81984073
• Mol file: 35958-51-1.mol

Synonyms:3,3'-dichloro-N,N'-diacetylbenzidine

Chemical Property of 3,3'-Dichloro-N,N'-diacetylbenzidine

Chemical Property:

• Melting Point: 302 °C(Solv: acetic acid (64-19-7))
• Boiling Point: 584.5±50.0 °C(Predicted)
• PKA: 13.54±0.70(Predicted)
• Flash Point: 307.3oC
• PSA: 65.18000
• Density: 1.377±0.06 g/cm3(Predicted)
• LogP: 5.87620
• XLogP3: 3.2
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 3
• Exact Mass: 336.0432331
• Heavy Atom Count: 22
• Complexity: 381

Purity/Quality:

99%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(=O)NC1=C(C=C(C=C1)C2=CC(=C(C=C2)NC(=O)C)Cl)Cl

Technology Process of 3,3'-Dichloro-N,N'-diacetylbenzidine

There total 4 articles about 3,3'-Dichloro-N,N'-diacetylbenzidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N,N'-Diacetylbenzidin (613-35-4) → N,N'-diacetyl-3,3'-dichlorobenzidine (35958-51-1)

Guidance literature:

With chlorine; acetic acid;

Reference yield:

3,3'-dichlorobenzidine (91-94-1) + acetic anhydride (108-24-7) → N,N'-diacetyl-3,3'-dichlorobenzidine (35958-51-1)

Guidance literature:

With sulfuric acid; acetic acid;

DOI:10.1039/j39710000762

Reference yield:

3,3'-dichlorobenzidine (91-94-1) + acetic anhydride (108-24-7) → N,N'-diacetyl-3,3'-dichlorobenzidine (35958-51-1) + N-acetyl-3,3'-dichlorobenzidine (72732-23-1)

Guidance literature:

With ethanol;

upstream raw materials:

N,N'-Diacetylbenzidin

ethanol

3,3'-dichlorobenzidine

acetic anhydride