Euphenol

Base Information

• Chemical Name: Euphenol
• CAS No.: 564-60-3
• Molecular Formula: C₃₀H₅₂O
• Molecular Weight: 428.742
• Mol file: 564-60-3.mol

Synonyms:

Chemical Property of Euphenol

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Dihydroeuphol ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Euphenol

There total 54 articles about Euphenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

tirucallol (79-63-0) → 24,25-dihydrolanosterol (79-62-9,564-60-3,6198-06-7,6593-55-1,13879-09-9,39701-94-5,59684-64-9,78821-82-6)

Guidance literature:

With 5%-palladium/activated carbon; hydrogen; In dichloromethane; at 20 ℃; for 24h; under 2585.81 Torr;

DOI:10.1016/j.jinorgbio.2014.03.017

Reference yield: 91.0%

dihydroagnosterol (2644-75-9) → 24,25-dihydrolanosterol (79-62-9,564-60-3,6198-06-7,6593-55-1,13879-09-9,39701-94-5,59684-64-9,78821-82-6)

Guidance literature:

With lithium; ethylamine; isopropylamine; In diethyl ether; at -78 ℃; for 5h;

DOI:10.1016/0040-4039(94)88450-1

Reference yield: 48.0%

15-oxolanost-8-en-3β-yl pivaloate (309958-24-5) → 24,25-dihydrolanosterol (79-62-9,564-60-3,6198-06-7,6593-55-1,13879-09-9,39701-94-5,59684-64-9,78821-82-6)

Guidance literature:

15-oxolanost-8-en-3β-yl pivaloate; With hydrazine hydrate; In diethylene glycol; at 150 ℃; for 4h;

With potassium hydroxide; In water; diethylene glycol; at 230 ℃; for 5h;

upstream raw materials:

diethyl ether

lanosterol

cholesterol

lanosterol

Downstream raw materials:

γ-lanosterol

lanost-8-en-3-one

3β-acetoxylanost-8-ene

C₆₄H₈₆O₆

Refernces

• 1、 Kang, Taek,Kim, Youngchan,Lee, Donggun,Wang, Zhen,Chang, Sukbok. "Iridium-catalyzed intermolecular amidation of sp3 C-H bonds: Late-stage functionalization of an unactivated methyl group". supporting information. p. 4141 - 4144. Retrieved 2014/04/03.
• 2、 Kavtaradze, Levan K.,Manley-Harris, Merilyn,Nicholson, Brian K.. "A low-toxicity method for the separation of lanosterol and dihydrolanosterol from commercial mixtures". . p. 697 - 700. Retrieved 2007/10/03.