Carbonic acid butyl 2-(p-iodobenzyl)butyl ester

Base Information

• Chemical Name: Carbonic acid butyl 2-(p-iodobenzyl)butyl ester
• CAS No.: 60075-86-7
• Molecular Formula: C₁₆H₂₃IO₃
• Molecular Weight: 390.261
• Hs Code.: 2920909090
• Mol file: 60075-86-7.mol

Synonyms:

Chemical Property of Carbonic acid butyl 2-(p-iodobenzyl)butyl ester

Chemical Property:

• Vapor Pressure: 1.53E-06mmHg at 25°C
• Boiling Point: 397.9°C at 760 mmHg
• Flash Point: 194.4°C
• PSA: 35.53000
• Density: 1.361g/cm³
• LogP: 4.81320

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Carbonic acid butyl 2-(p-iodobenzyl)butyl ester

There total 4 articles about Carbonic acid butyl 2-(p-iodobenzyl)butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzaldehyde (100-52-7) → Carbonic acid butyl ester 2-(4-iodo-benzyl)-butyl ester (60075-86-7)

Guidance literature:

Multi-step reaction with 4 steps

1: nPrCO₂K

2: H₂, aq. NaOH / Pd-C

4: (i) toluene, (ii) /BRN= 969148/, Py, CHCl₃

With sodium hydroxide; hydrogen; potassium n-butyrate; palladium on activated charcoal;

DOI:10.1021/jm00234a002

Reference yield:

ethyl 3-phenylpropenoic acid (620-78-0) → Carbonic acid butyl ester 2-(4-iodo-benzyl)-butyl ester (60075-86-7)

Guidance literature:

Multi-step reaction with 3 steps

1: H₂, aq. NaOH / Pd-C

3: (i) toluene, (ii) /BRN= 969148/, Py, CHCl₃

With sodium hydroxide; hydrogen; palladium on activated charcoal;

DOI:10.1021/jm00234a002

Reference yield:

1-(phenylmethyl)butanoic acid (56640-46-1,58635-83-9,89496-36-6,5669-16-9) → Carbonic acid butyl ester 2-(4-iodo-benzyl)-butyl ester (60075-86-7)

Guidance literature:

Multi-step reaction with 2 steps

2: (i) toluene, (ii) /BRN= 969148/, Py, CHCl₃

DOI:10.1021/jm00234a002

upstream raw materials:

phosgene

2-(p-iodobenzyl)butanol

butan-1-ol

1-(phenylmethyl)butanoic acid