Technology Process of boron(+3) cation, thallium(+1) cation, tetrafluoride
There total 11 articles about boron(+3) cation, thallium(+1) cation, tetrafluoride which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
In
solid;
byproducts: BF3; pyrolisis under Ar without solvent at 100-150°; TlBF4 identified by IR spectrum and comparison of m.p. with that of an authentic sample;
- Guidance literature:
-
In
acetone;
Tl deriv. was heated under reflux for 30 min; evapd.; residue treated with a hot benzene-EtOH (9:1), evapd., ppt. filtered off, washed with benzene and dried in vacuo at 50°/1 mm Hg; identified by IR spectrum and comparison of m.p. with that of authentic sample;
- Guidance literature:
-
In
water;
Tl2CO3 neutralized with 35% aq. HBF4 soln. in a Pt vessel;; recrystd. from hot water under slow cooling;;
