Butanamide, N,N'-(3,3'-dimethoxy(1,1'-biphenyl)-4,4'-diyl)bis(3-oxo-

Base Information

• Chemical Name: Butanamide, N,N'-(3,3'-dimethoxy(1,1'-biphenyl)-4,4'-diyl)bis(3-oxo-
• CAS No.: 4104-12-5
• Molecular Formula: C22H24 N2 O6
• Molecular Weight: 412.442
• Hs Code.: 2924299090
• European Community (EC) Number: 223-873-1
• NSC Number: 60665
• UNII: D3ATW3WC6W
• DSSTox Substance ID: DTXSID9063299
• Nikkaji Number: J116.795B
• Wikidata: Q81990641
• Mol file: 4104-12-5.mol

Synonyms:D3ATW3WC6W;4104-12-5;4',4'''-Bi-O-acetoacetanisidide;NSC-60665;4,4'-BIS(ACETOACETAMIDO)-3,3'-DIMETHOXYBIPHENYL;Butanamide, N,N'-(3,3'-dimethoxy(1,1'-biphenyl)-4,4'-diyl)bis(3-oxo-;Butanamide, N,N'-(3,3'-dimethoxy[1,1'-biphenyl]-4,4'-diyl)bis[3-oxo-;N,N'-(3,3'-Dimethoxy(1,1'-biphenyl)-4,4'-diyl)bis(3-oxobutyramide);NSC60665;UNII-D3ATW3WC6W;N,N'-Diacetoacetyldianisidine;DTXSID9063299;SCHEMBL11222052;EINECS 223-873-1;NSC 60665;AKOS024428980;O-BUTYRANISIDIDE, 4',4''-BIS(3-OXO-;Butanamide,N'-(3,3'-dimethoxy[1,1'-biphenyl]-4,4'-diyl)bis[3-oxo-;N,N'-(3,3'-DIMETHOXY(1,1'-BIPHENYL)-4,4'-DIYL)BIS(3-OXOBUTANAMIDE)

Chemical Property of Butanamide, N,N'-(3,3'-dimethoxy(1,1'-biphenyl)-4,4'-diyl)bis(3-oxo-

Chemical Property:

• Boiling Point: 632.9°Cat760mmHg
• Flash Point: 336.6°C
• PSA: 110.80000
• Density: 1.253g/cm³
• LogP: 3.35200
• XLogP3: 2.7
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 6
• Rotatable Bond Count: 9
• Exact Mass: 412.16343649
• Heavy Atom Count: 30
• Complexity: 583

Purity/Quality:

99% ^*data from raw suppliers

4,4'-BIS(ACETOACETAMIDO)-3,3'-DIMETHOXYBIPHENYL Aldrich ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(=O)CC(=O)NC1=C(C=C(C=C1)C2=CC(=C(C=C2)NC(=O)CC(=O)C)OC)OC

Technology Process of Butanamide, N,N'-(3,3'-dimethoxy(1,1'-biphenyl)-4,4'-diyl)bis(3-oxo-

There total 2 articles about Butanamide, N,N'-(3,3'-dimethoxy(1,1'-biphenyl)-4,4'-diyl)bis(3-oxo- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,3'-dimethoxy-(1,1'-biphenyl)-4,4'-diamine (119-90-4) + ethyl acetoacetate (141-97-9) → 4,4'-Bis-acetoacetylamino-3,3'-dimethoxy-biphenyl (4104-12-5)

Guidance literature:

With nitrobenzene; at 170 - 180 ℃;

Reference yield:

→ 4,4'-Bis-acetoacetylamino-3,3'-dimethoxy-biphenyl (4104-12-5)

Guidance literature:

o-Dianisidin, Diketen;

Reference yield:

N,N-Bis-(3-formamidopropyl)methylamine (40948-33-2) + 4-methoxy-3-nitrobenzyl chloride (6378-19-4) + 4,4'-Bis-acetoacetylamino-3,3'-dimethoxy-biphenyl (4104-12-5) → C52H76N12O8(2+)*2Cl(1-)

Guidance literature:

Multi-step reaction with 2 steps

2: hydrogenchloride / Heating

With hydrogenchloride;

upstream raw materials:

3,3'-dimethoxy-(1,1'-biphenyl)-4,4'-diamine

ethyl acetoacetate