Technology Process of methyl 3-(2-octadecylcyclopropen--1-yl)pentanoate
There total 5 articles about methyl 3-(2-octadecylcyclopropen--1-yl)pentanoate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: n-butyllithium / diethyl ether; hexane / 1 h / 0 °C
2: hexamethylphosphordiamide / Ambient temperature
3: 40 percent / dimethylsulfoxide
4: 1.) aq. NaOH, 2.) HCl / 1.) ethanol
5: TBAH / CH2Cl2
With
hydrogenchloride; N,N,N,N,N,N-hexamethylphosphoric triamide; sodium hydroxide; n-butyllithium; tetra(n-butyl)ammonium hydroxide;
In
diethyl ether; hexane; dichloromethane; dimethyl sulfoxide;
DOI:10.1016/0009-3084(94)02315-8
- Guidance literature:
-
Multi-step reaction with 4 steps
1: hexamethylphosphordiamide / Ambient temperature
2: 40 percent / dimethylsulfoxide
3: 1.) aq. NaOH, 2.) HCl / 1.) ethanol
4: TBAH / CH2Cl2
With
hydrogenchloride; N,N,N,N,N,N-hexamethylphosphoric triamide; sodium hydroxide; tetra(n-butyl)ammonium hydroxide;
In
dichloromethane; dimethyl sulfoxide;
DOI:10.1016/0009-3084(94)02315-8
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 40 percent / dimethylsulfoxide
2: 1.) aq. NaOH, 2.) HCl / 1.) ethanol
3: TBAH / CH2Cl2
With
hydrogenchloride; sodium hydroxide; tetra(n-butyl)ammonium hydroxide;
In
dichloromethane; dimethyl sulfoxide;
DOI:10.1016/0009-3084(94)02315-8
