CADION

Base Information

• Chemical Name: CADION
• CAS No.: 5392-67-6
• Molecular Formula: C18H14N6O2
• Molecular Weight: 346.348
• Hs Code.: 2928000090
• Mol file: 5392-67-6.mol

Synonyms:1-Triazene,1-(4-nitrophenyl)-3-[4-(phenylazo)phenyl]- (9CI);Triazene,1-(p-nitrophenyl)-3-[p-(phenylazo)phenyl]- (6CI,7CI,8CI);1-(4-Nitrophenyl)-3-(4-phenylazophenyl)triazene;1-(p-Nitrophenyl)-3-(p'-azobenzene)triazene;3-(p-Nitrophenyl)-1-[p-(phenylazo)phenyl]triazene;Cadion;Cadion A;NSC 6282;NSC 66456;p-Nitrophenyldiazoaminoazobenzene;

Chemical Property of CADION

Chemical Property:

• Vapor Pressure: 1.6E-11mmHg at 25°C
• Melting Point: 189 °C (dec.)(lit.)
• Refractive Index: 1.666
• Boiling Point: 535 °C at 760 mmHg
• PKA: -0.93±0.50(Predicted)
• Flash Point: 277.4 °C
• PSA: 107.29000
• Density: 1.3 g/cm³
• LogP: 6.71720

Purity/Quality:

99.0% ^*data from raw suppliers

Cadion for spectrophotometric det. of Cd, Ni, ≥98.0% ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xn
• Hazard Codes: Xn
• Statements: 5-22-43
• Safety Statements: 14-15-36/37

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

Technology Process of CADION

There total 1 articles about CADION which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 1-(4-nitrophenyl)-3-(4-phenylazophenyl)triazene (5392-67-6)

Guidance literature:

Reference yield: 35.0%

pyridine (110-86-1) + N-(4-nitro-phenyl)-N'-(4-phenylazo-phenyl)-triazene (5392-67-6) + mercury(II) diacetate (1600-27-7) → [bis-(3-(4-phenyldiazophenyl)-1-(4-nitrophenyl)triazenide)(bispyridinyl)-mercury(II)]

Guidance literature:

With KOH; In methanol; acetone; under N2 atm.to soln. ligand in acetone soln. KOH in MeOH was added, soln. Hg(OAc)2 in acetone was added and stirred for 2 h, ppt. was filtered,washed with acetone and dried in vacuo, dissolved in THF-pyridine; slow evapn. at room temp. for 24 h;

DOI:10.1016/j.ica.2006.07.032

Reference yield:

N-(4-nitro-phenyl)-N'-(4-phenylazo-phenyl)-triazene (5392-67-6) + silver(I) acetate (563-63-3) → Ag(1+)*C18H13N6O2(1-)={AgC18H13N6O2}

Guidance literature:

In pyridine; methanol; acetone; pptd. by methanol; pptd. from pyridine by methanol;

Refernces