Technology Process of Indicine N-oxide
There total 13 articles about Indicine N-oxide which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 9.3 percent / camphorsulfonic acid / benzene / 72 h / Heating
2: 1) DCC, DMAP, 2) 1 M HCl / 1) toluene, r.t., 6 d, 2) r.t., 28 h
3: 81 percent / m-chloroperoxybenzoic acid / acetone / 2 h / Ambient temperature
With
hydrogenchloride; dmap; 3-chloro-benzenecarboperoxoic acid; dicyclohexyl-carbodiimide;
camphor-10-sulfonic acid;
In
acetone; benzene;
DOI:10.1016/S0040-4020(01)80345-8
- Guidance literature:
-
Multi-step reaction with 3 steps
1: concd hydrochloric acid / Ambient temperature
2: 1.) DCC, DMAP; 2.) 0.6 M HCl / 1.) toluene, r.t., 3 d; 2.) r.t., 8 h
3: MCPBA / acetone / 1 h / Ambient temperature
With
hydrogenchloride; dmap; 3-chloro-benzenecarboperoxoic acid; dicyclohexyl-carbodiimide;
In
acetone;
DOI:10.1246/bcsj.60.4107
