4,5-Dihydro-2-((phenylmethyl)thio)-(1H)imidazole

Base Information

• Chemical Name: 4,5-Dihydro-2-((phenylmethyl)thio)-(1H)imidazole
• CAS No.: 20268-38-6
• Molecular Formula: C10H12N2S
• Molecular Weight: 192.285
• Hs Code.: 2933290090
• Mol file: 20268-38-6.mol

Synonyms:2-(Benzylsulfanyl)-4,5-dihydro-1H-imidazole;4,5-Dihydro-2-((phenylmethyl)thio)-(1H)imidazole;

Chemical Property of 4,5-Dihydro-2-((phenylmethyl)thio)-(1H)imidazole

Chemical Property:

• Vapor Pressure: 0.000378mmHg at 25°C
• Melting Point: 68-70 °C
• Refractive Index: 1.635
• Boiling Point: 317.7 °C at 760 mmHg
• PKA: 8.85±0.40(Predicted)
• Flash Point: 145.9 °C
• PSA: 49.69000
• Density: 1.19 g/cm³
• LogP: 1.64340

Purity/Quality:

99% ^*data from raw suppliers

4,5-DIHYDRO-2-((PHENYLMETHYL)THIO)-(1H)IMIDAZOLE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4,5-Dihydro-2-((phenylmethyl)thio)-(1H)imidazole

There total 2 articles about 4,5-Dihydro-2-((phenylmethyl)thio)-(1H)imidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N,N'-ethylenethiourea (96-45-7) + benzyl chloride (100-44-7) → S-benzyl-N,N'-ethyleneisothiourea (20268-38-6)

Guidance literature:

With ethanol;

DOI:10.1021/ja01146a030 DOI:10.1021/ja01633a068 DOI:10.1021/ja01151a511 DOI:10.1039/jr9490001996

Reference yield:

→ S-benzyl-N,N'-ethyleneisothiourea (20268-38-6)

Guidance literature:

Imidazolinthiol-(2) u. Benzylchlorid in Me./Siedetemp.;

Reference yield:

S-benzyl-N,N'-ethyleneisothiourea (20268-38-6) + 5-isopropyl-1,3-cyclohexanedione (18456-87-6) → 5-(1-methylethyl)-2-(2-imidazolidinylidene)-1,3-cyclohexanedione

Guidance literature:

With 1,4-diaza-bicyclo[2.2.2]octane; hydrogenchloride; In dichloromethane; ethyl acetate;

upstream raw materials:

N,N'-ethylenethiourea

benzyl chloride