1,4-Bis(3-aminopropoxy)butane

Base Information

• Chemical Name: 1,4-Bis(3-aminopropoxy)butane
• CAS No.: 7300-34-7
• Deprecated CAS: 1352480-53-5,1425008-15-6
• Molecular Formula: C12H24N2O2
• Molecular Weight: 204.313
• Hs Code.: 2922199090
• European Community (EC) Number: 230-745-9
• NSC Number: 36635
• DSSTox Substance ID: DTXSID0064622
• Nikkaji Number: J60.717G
• Wikidata: Q72444177
• Mol file: 7300-34-7.mol

Synonyms:4,9-dioxa-1,12-dodecanediamine;DO-DA cpcd

Chemical Property of 1,4-Bis(3-aminopropoxy)butane

Chemical Property:

• Appearance/Colour: CLEAR COLOURLESS LIQUID
• Vapor Pressure: 1 hPa (50 °C)
• Melting Point: 4.5oC
• Refractive Index: n20/D 1.462
• Boiling Point: 294.9°Cat760mmHg
• PKA: 10.06±0.10(Predicted)
• Flash Point: 138.6°C
• PSA: 70.50000
• Density: 0.956g/cm³
• LogP: 1.89800
• Storage Temp.: Store below +30°C.
• Water Solubility.: Completely miscible in water
• XLogP3: -0.5
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 11
• Exact Mass: 204.183778013
• Heavy Atom Count: 14
• Complexity: 90.1

Purity/Quality:

98% ^*data from raw suppliers

1,4-Butanediol Bis(3-aminopropyl) Ether ^*data from reagent suppliers

Safty Information:

• Pictogram(s): A poison by skin contact. Moderately toxic by ingestion and inhalation.
• Hazard Codes: T
• Statements: 23-34-24
• Safety Statements: 26-36/37/39-45

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

• Canonical SMILES: C(CCOCCCN)COCCCN
• Uses: 1,4-Butanediol Bis(3-Aminopropyl)ether is used in method for preparing Mannich base for use as epoxy resin curative, and method for preparing cured epoxy resin.

Technology Process of 1,4-Bis(3-aminopropoxy)butane

There total 6 articles about 1,4-Bis(3-aminopropoxy)butane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

→ 4,9-dioxa-1,12-dodecanediamine (7300-34-7,72088-96-1) + oxalic acid diethyl ester (95-92-1)

Guidance literature:

Reference yield:

butanediol bis-(propionitrile)ether (18664-94-3) → 4,9-dioxa-1,12-dodecanediamine (7300-34-7,72088-96-1)

Guidance literature:

With ammonia; nickel; at 100 ℃; under 73550.8 Torr; Hydrogenation;

Reference yield:

3,3'-(but-2-yne-1,4-diylbis(oxy))dipropanenitrile (90918-31-3) → 4,9-dioxa-1,12-dodecanediamine (7300-34-7,72088-96-1)

Guidance literature:

With ammonia; nickel; at 100 ℃; under 73550.8 Torr; Hydrogenation;

upstream raw materials:

butanediol bis-(propionitrile)ether

3,3'-(but-2-yne-1,4-diylbis(oxy))dipropanenitrile

ammonia

Downstream raw materials:

N-{3-[4-(3-Amino-propoxy)-butoxy]-propyl}-benzamide

Refernces

• 1、 -. "PROCESS FOR THE PRODUCTION OF ETHER ISOCYANATES BACKGROUND OF THE INVENTION". . . Retrieved 2008/06/13.
• 2、 -. "Precursor to nucleic acid probe". . . Retrieved 2008/06/13.