TETRAHYDROLINALOOL

Base Information

• Chemical Name: TETRAHYDROLINALOOL
• CAS No.: 57706-88-4
• Molecular Formula: C10H22O
• Molecular Weight: 158.28100
• Mol file: 57706-88-4.mol

Synonyms:3-Octanol, 3,7-dimethyl-, (±)-;

Chemical Property of TETRAHYDROLINALOOL

Chemical Property:

• Vapor Pressure: 0.115mmHg at 25°C
• Melting Point: 31.5°C
• Refractive Index: n20/D 1.434(lit.)
• Boiling Point: 194.5oC at 760mmHg
• Flash Point: 76.1oC
• PSA: 20.23000
• Density: 0.826g/cm3
• LogP: 2.97370

Purity/Quality:

98.5% ^*data from raw suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26-36

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of TETRAHYDROLINALOOL

There total 50 articles about TETRAHYDROLINALOOL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

2,6-dimethyl-6-(triphenylsilyloxy)octane → tetrahydrolinalool (78-69-3,57706-88-4)

Guidance literature:

With naphthalene; lithium; In tetrahydrofuran; methanol; at 20 ℃; for 5h;

DOI:10.1016/j.tet.2005.03.145

Reference yield: 94.0%

6-Methoxymethoxy-2,6-dimethyl-octane (144708-84-9) → tetrahydrolinalool (78-69-3,57706-88-4)

Guidance literature:

With methanol; DOWEX-50W-X₂; for 2h; Heating;

DOI:10.1080/00397919208021548

Reference yield: 93.0%

3,7-dimethylocta-1,6-dien-3-ol (78-70-6) → tetrahydrolinalool (78-69-3,57706-88-4)

Guidance literature:

With ammonium chloride; In methanol; Electrochemical reaction;

DOI:10.1016/S0040-4039(03)01035-9

upstream raw materials:

linalool

3,7-dimethylocta-1,6-dien-3-ol

3-methyl-1-butyl acetate

ethylmagnesium bromide

Downstream raw materials:

(S)-(-)-Tetrahydrolinalylphenylether

Refernces

• 1、 Barbier,Locquin. "-". . . Retrieved 1914.
• 2、 Diler, Fatma,Burhan, Hakan,Genc, Hayriye,Kuyuldar, Esra,Zengin, Mustafa,Cellat, Kemal,Sen, Fatih. "Efficient preparation and application of monodisperse palladium loaded graphene oxide as a reusable and effective heterogeneous catalyst for suzuki cross-coupling reaction". . . Retrieved 2019/11/29.
• 3、 Friedfeld, Max R.,Margulieux, Grant W.,Schaefer, Brian A.,Chirik, Paul J.. "Bis(phosphine)cobalt dialkyl complexes for directed catalytic alkene hydrogenation". supporting information. p. 13178 - 13181. Retrieved 2015/03/30.