Technology Process of BenzeneMethanaMine, N,N-diMethyl-α-[2-(1-naphthalenyloxy)ethyl]-
There total 21 articles about BenzeneMethanaMine, N,N-diMethyl-α-[2-(1-naphthalenyloxy)ethyl]- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
(S)-(+)-3-(dimethylamino)-3-phenyl-1-propanol;
With
sodium hydride;
In
N,N-dimethyl acetamide;
at 65 ℃;
for 1.5h;
Inert atmosphere;
Large scale;
1-Fluoronaphthalene;
In
N,N-dimethyl acetamide;
at 100 ℃;
for 7h;
Inert atmosphere;
Large scale;
With
ethanol; acetyl chloride;
In
ethyl acetate;
at 20 ℃;
for 6h;
Concentration;
Temperature;
Reagent/catalyst;
Solvent;
Large scale;
- Guidance literature:
-
With
hydrogenchloride;
In
Isopropyl acetate;
Solvent;
Cooling with ice;
- Guidance literature:
-
(R)-(-)-3-(1-naphthalenyloxy)-1-phenyl-1-propanol;
With
dmap; methanesulfonyl chloride; triethylamine;
In
tetrahydrofuran;
at 0 ℃;
for 4h;
N,N-dimethylammonium chloride;
In
tetrahydrofuran;
at 40 ℃;
for 25h;
Temperature;