ASISCHEM D29201

Base Information

• Chemical Name: ASISCHEM D29201
• CAS No.: 928707-94-2
• Molecular Formula: C15H17NO2
• Molecular Weight: 0
• Mol file: 928707-94-2.mol

Synonyms:ASISCHEM D29201;2-(2,5-DIMETHYL-1H-PYRROL-1-YL)-BENZOIC ACID ETHYL ESTER;BENZOIC ACID, 2-(2,5-DIMETHYL-1H-PYRROL-1-YL)-, ETHYL ESTER

Chemical Property of ASISCHEM D29201

Chemical Property:

• PSA: 31.23000
• LogP: 3.27080

Purity/Quality:

99% ^*data from raw suppliers

2-(2,5-DIMETHYL-1H-PYRROL-1-YL)-BENZOIC ACID ETHYL ESTER 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of ASISCHEM D29201

There total 1 articles about ASISCHEM D29201 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

2,5-hexanedione (110-13-4) + 2-ethoxycarbonylaniline (87-25-2) → ethyl 2-(2,5-dimethyl-1-pyrrol-1-yl)benzoate (928707-94-2)

Guidance literature:

In acetic acid; for 1h; Inert atmosphere; Reflux;

DOI:10.1007/s11172-009-0060-0

Reference yield: 83.5%

ethyl 2-(2,5-dimethyl-1-pyrrol-1-yl)benzoate (928707-94-2) → [2-(2,5-dimethyl-1H-pyrrol-1-yl)phenyl]methanol (97690-10-3)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether; at 0 - 20 ℃; for 1h; Inert atmosphere;

DOI:10.1007/s11172-009-0060-0

upstream raw materials:

2,5-hexanedione

2-ethoxycarbonylaniline

Downstream raw materials:

[2-(2,5-dimethyl-1H-pyrrol-1-yl)phenyl]methanol

Refernces