Benzyldichlorophosphine

Base Information Edit

Chemical Name:Benzyldichlorophosphine
CAS No.:4545-85-1
Molecular Formula:C7H7Cl2P
Molecular Weight:193.012
Hs Code.:
Mol file:4545-85-1.mol

Synonyms:Benzyldichlorophosphine

Suppliers and Price of Benzyldichlorophosphine

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of Benzyldichlorophosphine Edit

Chemical Property:

Boiling Point:110-111 °C(Press: 12 Torr)
PSA：13.59000
Density:1.300 g/cm3
LogP:3.97610

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Benzyldichlorophosphine

There total 11 articles about Benzyldichlorophosphine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 14990-01-3
benzylphosphine

: 4545-85-1
benzyldichlorophosphane

Guidance literature:: With COCl₂; In chloroform; at -30 ℃; for 3h;

Reference yield: 40.0%

: 100-39-0
benzyl bromide

: 4545-85-1
benzyldichlorophosphane

Guidance literature:: benzyl bromide; With magnesium; In diethyl ether; at 20 ℃; for 2h; Inert atmosphere; Reflux;

With zinc(II) chloride; In diethyl ether; at 0 - 20 ℃; for 0.25h; Inert atmosphere;

With phosphorus trichloride; In diethyl ether; at 45 ℃; for 1h; Inert atmosphere; Reflux;
DOI:10.1021/acs.inorgchem.1c02734

Reference yield:

: 4545-85-1
benzyldichlorophosphane

Guidance literature:: benzyl halide; With magnesium; In diethyl ether; Heating;

With cadmium(II) chloride; at 0 ℃;

With phosphorus trichloride; In diethyl ether; at 20 ℃;
DOI:10.1002/1522-2675(200208)85:8<2503::AID-HLCA2503>3.0.CO;2-I