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Methyl 4,4-dimethyl-2-[(trifluoromethylsulfonyl)oxy]cyclohex-1-ene-1-carboxylate

Base Information Edit
  • Chemical Name:Methyl 4,4-dimethyl-2-[(trifluoromethylsulfonyl)oxy]cyclohex-1-ene-1-carboxylate
  • CAS No.:1228780-46-8
  • Molecular Formula:C11H15F3O5S
  • Molecular Weight:316.298
  • Hs Code.:
  • Mol file:1228780-46-8.mol
Methyl 4,4-dimethyl-2-[(trifluoromethylsulfonyl)oxy]cyclohex-1-ene-1-carboxylate

Synonyms:Methyl 4,4-dimethyl-2-[(trifluoromethylsulfonyl)oxy]cyclohex-1-ene-1-carboxylate;4,4-dimethyl-2-[[(trifluoromethyl)sulfonyl]oxy]-1-cyclohexene-1-carboxylic acid methyl ester

Suppliers and Price of Methyl 4,4-dimethyl-2-[(trifluoromethylsulfonyl)oxy]cyclohex-1-ene-1-carboxylate
Supply Marketing:Edit
Business phase:
The product has achieved commercial mass production*data from LookChem market partment
Manufacturers and distributors:
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Total 2 raw suppliers
Chemical Property of Methyl 4,4-dimethyl-2-[(trifluoromethylsulfonyl)oxy]cyclohex-1-ene-1-carboxylate Edit
Chemical Property:
Purity/Quality:

99% *data from raw suppliers

Safty Information:
  • Pictogram(s):  
  • Hazard Codes: 
MSDS Files:

SDS file from LookChem

Useful:
Technology Process of Methyl 4,4-dimethyl-2-[(trifluoromethylsulfonyl)oxy]cyclohex-1-ene-1-carboxylate

There total 3 articles about Methyl 4,4-dimethyl-2-[(trifluoromethylsulfonyl)oxy]cyclohex-1-ene-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
methyl 4,4-dimethyl-2-oxocyclohexancarboxylate; With sodium hydride; In dichloromethane; at 0 ℃; for 0.833333h;
trifluoromethylsulfonic anhydride; In dichloromethane; at -78 - 20 ℃;
Guidance literature:
methyl 4,4-dimethyl-2-oxocyclohexancarboxylate; With sodium hydride; In dichloromethane; at 0 ℃;
trifluoroacetic anhydride; In dichloromethane; at -78 - 20 ℃;
Guidance literature:
Multi-step reaction with 2 steps
1.1: sodium hydride / tetrahydrofuran / Reflux; Inert atmosphere
1.2: 4 h / Reflux
2.1: sodium hydride / dichloromethane / 0.83 h / 0 °C
2.2: -78 - 20 °C
With sodium hydride; In tetrahydrofuran; dichloromethane;
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