9-CHLORO-6,7-DIMETHOXY-3-NITROACRIDINE

Base Information

• Chemical Name: 9-CHLORO-6,7-DIMETHOXY-3-NITROACRIDINE
• CAS No.: 6628-92-8
• Molecular Formula: C₁₅H₁₁ClN₂O₄
• Molecular Weight: 318.716
• Mol file: 6628-92-8.mol

Synonyms:9-Chlor-2,3-dimethoxy-6-nitro-acridin;9-chloro-2,3-dimethoxy-6-nitro-acridine;2,3-Dimethoxy-9-chlor-6-nitroacridin;2,3-dimethoxy-9-chloro-6-nitroacridine;

Chemical Property of 9-CHLORO-6,7-DIMETHOXY-3-NITROACRIDINE

Chemical Property:

• Vapor Pressure: 5.72E-10mmHg at 25°C
• Refractive Index: 1.686
• Boiling Point: 508.8 °C at 760 mmHg
• Flash Point: 261.5 °C
• PSA: 77.17000
• Density: 1.431 g/cm³
• LogP: 4.49000

Purity/Quality:

99% ^*data from raw suppliers

9-CHLORO-6,7-DIMETHOXY-3-NITROACRIDINE Aldrich ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

Technology Process of 9-CHLORO-6,7-DIMETHOXY-3-NITROACRIDINE

There total 5 articles about 9-CHLORO-6,7-DIMETHOXY-3-NITROACRIDINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 2,3-dimethoxy-9-chloro-6-nitroacridine (6628-92-8)

Guidance literature:

With toluene; trichlorophosphate;

Reference yield:

2-(3,4-dimethoxy-anilino)-4-nitro-benzoic acid (7159-41-3) → 2,3-dimethoxy-9-chloro-6-nitroacridine (6628-92-8)

Guidance literature:

With trichlorophosphate;

DOI:10.1021/jo01164a019

Reference yield:

2-chloro-4-nitrobenzoic acid (99-60-5) → 2,3-dimethoxy-9-chloro-6-nitroacridine (6628-92-8)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate; copper; amyl alcohol

2: phosphoryl chloride

With pentan-1-ol; copper; potassium carbonate; trichlorophosphate;

DOI:10.1021/jo01164a019

upstream raw materials:

2-(3,4-dimethoxy-anilino)-4-nitro-benzoic acid

2-chloro-4-nitrobenzoic acid

3,4-dimethoxyaniline

Downstream raw materials:

1-diethylamino-3-(2,3-dimethoxy-6-nitro-acridin-9-ylamino)-propan-2-ol