Cyclothizenovnadium dibromide

Base Information

• Chemical Name: Cyclothizenovnadium dibromide
• CAS No.: 100286-36-0
• Molecular Formula: Br2H2N3S2V
• Molecular Weight: 316.89
• Mol file: 100286-36-0.mol

Synonyms:Cyclothizenovnadium dibromide

Chemical Property of Cyclothizenovnadium dibromide

Chemical Property:

• PSA: 114.68000
• LogP: 1.30980

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Cyclothizenovnadium dibromide

There total 1 articles about Cyclothizenovnadium dibromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

vanadium(III) bromide (13470-26-3) + tetrasulfur tetranitride (28950-34-7) → {VBr2(N3S2)}(n) (100286-36-0)

Guidance literature:

In further solvent(s); byproducts: S2Br2, S, N2; refluxing VBr3 (6.16 mmol) and S4N4 (6.13 mmol) in CH2Br2 for 6 h; cooling down to room temp.;; pptn.; filtering over frit and washing twice with CH2Br2; drying in vac.; recrystn. from CH2Br2, layering with hexane, storage at 0°C for 3 d; elem. anal.;;

upstream raw materials:

vanadium(III) bromide

tetrasulfur tetranitride

Refernces