3-chloro-4-(trifluoroMethyl)benzene-1-sulfonyl chloride

Base Information

• Chemical Name: 3-chloro-4-(trifluoroMethyl)benzene-1-sulfonyl chloride
• CAS No.: 132481-85-7
• Molecular Formula: C7H3Cl2F3O2S
• Molecular Weight: 279.0637296
• Hs Code.: 2904909090
• Mol file: 132481-85-7.mol

Synonyms:3-chloro-4-(trifluoroMethyl)benzene-1-sulfonyl chloride;3-Chloro-4-(trifluoromethyl)benzenesulphonylchloride

Chemical Property of 3-chloro-4-(trifluoroMethyl)benzene-1-sulfonyl chloride

Chemical Property:

• Vapor Pressure: 0.002mmHg at 25°C
• Boiling Point: 299.623°C at 760 mmHg
• Flash Point: 135.007°C
• PSA: 42.52000
• Density: 1.627g/cm³
• LogP: 4.36710

Purity/Quality:

97% ^*data from raw suppliers

3-Chloro-4-(trifluoromethyl)benzenesulfonyl chloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-chloro-4-(trifluoroMethyl)benzene-1-sulfonyl chloride

There total 1 articles about 3-chloro-4-(trifluoroMethyl)benzene-1-sulfonyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 3-chloro-4-(trifluoromethyl)benzenesulfonyl chloride (132481-85-7)

Guidance literature:

Reference yield: 83.0%

1-ethylpyrrolidine (7335-06-0) + 3-chloro-4-(trifluoromethyl)benzenesulfonyl chloride (132481-85-7) → 1-((3-chloro-4-(trifluoromethyl)phenyl)sulfonyl)pyrrolidine

Guidance literature:

With tert.-butylhydroperoxide; tetra-(n-butyl)ammonium iodide; In tetrahydrofuran; decane; at 80 ℃; for 4h; chemoselective reaction; Sealed tube;

DOI:10.1039/c8ob02992j

Reference yield: 74.0%

3-chloro-4-(trifluoromethyl)benzenesulfonyl chloride (132481-85-7) → 3-chloro-4-(trifluoromethyl)benzene-1-sulfonyl hydrazide

Guidance literature:

With hydrazine hydrate; In tetrahydrofuran; at 0 ℃; for 1h;

DOI:10.1021/acs.joc.9b02646

Refernces