Technology Process of Stibine, iodothioxo-
There total 4 articles about Stibine, iodothioxo- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
In
neat (no solvent);
reaction sets in at normal temp.; mildly heated to complete reaction;; SbI3 is removed by extraction with boiling CS2;;
- Guidance literature:
-
With
hydrogen iodide;
In
not given;
a soln. of SbI3 in HI soln. is pptd. by H2S soln. (also in HI soln.), H2O added and the mixt. shaken for 8h at 18°C;; decanting, washing with tartaric acid soln., then with water;;
- Guidance literature:
-
In
melt;
powdered Sb2S3 is dissolved in melting SbI3;; solidified mass is freed from excess of SbI3 with dild. HCl;;