1,4-DISILABUTANE

Base Information

• Chemical Name: 1,4-DISILABUTANE
• CAS No.: 4364-07-2
• Molecular Formula: C2H10Si2
• Molecular Weight: 90.2724
• Hs Code.: 2931900090
• Mol file: 4364-07-2.mol

Synonyms:1,4-Disilabutane(6CI,7CI,8CI);1,2-Bis(silyl)ethane;1,2-Bis(trihydrosilyl)ethane;1,2-Disilylethane;

Chemical Property of 1,4-DISILABUTANE

Chemical Property:

• Melting Point: -15°C
• Refractive Index: 1.4141
• Boiling Point: 54.5 °C at 760 mmHg
• Flash Point: -31°'C (-24°F)
• PSA: 0.00000
• Density: 0,697 g/cm3
• LogP: -1.44620

Purity/Quality:

98%,99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s): F
• Hazard Codes: F
• Statements: 5
• Safety Statements: 16-36

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,4-DISILABUTANE

There total 4 articles about 1,4-DISILABUTANE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

1,2-bis(trichlorosilyl)ethane (2504-64-5) → 1,4-disilabutane (4364-07-2)

Guidance literature:

With lithium aluminium tetrahydride; In dibutyl ether; at 80 - 100 ℃; for 4h;

Reference yield: 85.0%

1,2-bis(trichlorosilyl)ethane (2504-64-5) + lithium hydride → 1,4-disilabutane (4364-07-2)

Guidance literature:

In not given;

Reference yield: 20.0%

(bromomethyl)silane (7570-21-0) → 1,4-disilabutane (4364-07-2) + CH5BrMgSi

Guidance literature:

With magnesium chloride; In tetrahydrofuran;

upstream raw materials:

1,2-bis(trichlorosilyl)ethane

(bromomethyl)silane

lithium aluminium tetrahydride

Downstream raw materials:

ethene

vinylsilane

acetylene

1,2-bis(trimethoxysilyl)-ethane

Refernces

• 1、 -. "CATALYST DEHYDROGENATIVE COUPLING OF CARBOSILANES WITH AMMONIA, AMNINES AND AMIDINES". Paragraph 00117-00118. . Retrieved 2016/10/27.
• 2、 Schmidbaur, Hubert,Doerzbach, Cornelia. "Synthesis and Characterization of Simple α-Sila- and α,ω-Disilaalkanes: Precursors for the CVD Production of Amorphous Silicon a-SiC:H". . p. 1088 - 1096. Retrieved 2007/10/02.