Technology Process of (2Z,7Z)-2,7-Nonadiene-1,9-diol
There total 4 articles about (2Z,7Z)-2,7-Nonadiene-1,9-diol which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
quinoline; hydrogen;
Lindlar's catalyst;
In
ethanol;
for 2h;
DOI:10.1021/ja00343a026
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 63 percent / 1.) n-butyllithium / diethyl ether; hexane; tetrahydrofuran / 1.) -13 deg C, 20 min, 2.) reflux, 2.25 h
2: 99 percent / quinoline, hydrogen / Lindlar's catalyst / ethanol / 2 h
With
quinoline; n-butyllithium; hydrogen;
Lindlar's catalyst;
In
tetrahydrofuran; diethyl ether; ethanol; hexane;
DOI:10.1021/ja00343a026
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 63 percent / n-BuLi / tetrahydrofuran / 48 h / Heating
2: 80 percent / p-TsOH / methanol / Heating
3: H2 / Lindlar cat. / ethyl acetate / 1520 Torr
With
n-butyllithium; hydrogen; toluene-4-sulfonic acid;
Lindlar catalyst;
In
tetrahydrofuran; methanol; ethyl acetate;
DOI:10.1016/S0040-4039(01)82101-8
