Tris-(2-hydroxyethyl)ammonium 2-methylphenoxyacetate

Base Information

• Chemical Name: Tris-(2-hydroxyethyl)ammonium 2-methylphenoxyacetate
• CAS No.: 55543-68-5
• Molecular Formula: C15H25NO6
• Molecular Weight: 315.367
• Mol file: 55543-68-5.mol

Synonyms:tris-(2-hydroxyethyl)ammonium 2-methylphenoxyacetate

Chemical Property of Tris-(2-hydroxyethyl)ammonium 2-methylphenoxyacetate

Chemical Property:

• Boiling Point: 288.4 °C at 760 mmHg
• Flash Point: 115.7 °C
• PSA: 110.46000
• LogP: -0.27630
• Hydrogen Bond Donor Count: 4
• Hydrogen Bond Acceptor Count: 6
• Rotatable Bond Count: 8
• Exact Mass: 315.16818752
• Heavy Atom Count: 22
• Complexity: 206

Purity/Quality:

99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=CC=CC=C1OCC(=O)[O-].C(CO)[NH+](CCO)CCO

Technology Process of Tris-(2-hydroxyethyl)ammonium 2-methylphenoxyacetate

There total 2 articles about Tris-(2-hydroxyethyl)ammonium 2-methylphenoxyacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.8%

o-methylphenoxyacetic acid (1878-49-5) + triethanolamine hydrochloride (637-39-8,67924-33-8) → 2-(2-methylphenyloxy)acetate of tris(2-hydroxyethyl)-ammonium (55543-68-5)

Guidance literature:

o-methylphenoxyacetic acid; for 1h; Reflux; Alkaline conditions;

triethanolamine hydrochloride; Reflux;

DOI:10.1134/S1070363218100353

Reference yield:

→ 2-(2-methylphenyloxy)acetate of tris(2-hydroxyethyl)-ammonium (55543-68-5)

Guidance literature:

Triethanolamin, o-Kresyloxyessigsaeure;

Reference yield: 98.0%

zinc chloride sesquihydrate + 2-(2-methylphenyloxy)acetate of tris(2-hydroxyethyl)-ammonium (55543-68-5) → (triethanolammonium o-methylphenoxyacetate)*ZnCl2

Guidance literature:

In methanol; soln. of Zn salt in MeOH added dropwise to soln. of cresacin in MeOH, mixt. stirred at 25°C for 12 h; evapn. under vac., solid washed with ether, dried under vac.;

DOI:10.1134/S107036320809017X

upstream raw materials:

o-methylphenoxyacetic acid

triethanolamine hydrochloride

Downstream raw materials:

C₈H₁₉NO₄Si*C₉H₁₀O₃

C₇H₁₇NO₄Si*C₉H₁₀O₃

Refernces