OCTAFLUOROADIPAMIDE

Base Information

• Chemical Name: OCTAFLUOROADIPAMIDE
• CAS No.: 355-66-8
• Molecular Formula: C6H4F8N2O2
• Molecular Weight: 288.097
• Hs Code.: 2924199090
• Mol file: 355-66-8.mol

Synonyms:OCTAFLUOROADIPAMIDE;OCTAFLUOROADIPOAMIDE;2,2,3,3,4,4,5,5-OCTAFLUOROHEXANEDIAMIDE;2,2,3,3,4,4,5,5-Octafluorohexanediamide 97%

Chemical Property of OCTAFLUOROADIPAMIDE

Chemical Property:

• Vapor Pressure: 0.000178mmHg at 25°C
• Melting Point: 240-242 °C (dec.)(lit.)
• Boiling Point: 329.4 °C at 760 mmHg
• Flash Point: 153 °C
• PSA: 86.18000
• Density: 1.665 g/cm³
• LogP: 1.89880

Purity/Quality:

99%, ^*data from raw suppliers

Octafluoroadipamide ^*data from reagent suppliers

Safty Information:

• Pictogram(s): C
• Hazard Codes: C,Xi
• Statements: 34
• Safety Statements: 26-36/37/39-45

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of OCTAFLUOROADIPAMIDE

There total 12 articles about OCTAFLUOROADIPAMIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,6-bis(fluorosulfato)perfluorhexane (85452-27-3) → octafluoro-adipic acid diamide (355-66-8)

Guidance literature:

With ammonia; In diethyl ether; water; at 35 ℃; for 5h;

DOI:10.1007/BF00952946

Reference yield:

perfluoroadipic acid (336-08-3) → octafluoro-adipic acid diamide (355-66-8)

Guidance literature:

Multi-step reaction with 3 steps

1: 200 °C

2: phosphorus (V)-chloride

3: dioxane; ammonia

With 1,4-dioxane; phosphorus pentachloride; ammonia;

DOI:10.1021/ja01642a080

Reference yield:

octafluoro-adipic acid ethyl ester chloride (376-51-2) → octafluoro-adipic acid diamide (355-66-8)

Guidance literature:

With 1,4-dioxane; ammonia;

DOI:10.1021/ja01642a080

upstream raw materials:

octafluoro-adipic acid ethyl ester chloride

diethyl perfluoroadipate

2,2,3,3,4,4,5,5-octafluoro-hexanediimidic acid dimethyl ester

1,6-bis(fluorosulfato)perfluorhexane

Downstream raw materials:

octafluoroadiponitrile

5-cyanoperfluoropentanoyl chloride

2,2,3,3,4,4,5,5-octafluorohexane-1,6-diamine

octafluoroadipoyl chloride

Refernces

• 1、 Fokin, A. V.,Rapkin, A. I.,Tatarinov, A. S.,Titov, V. A.,Studnev, Yu. N.. "REACTION OF POLYFLUOROALKYL FRUOROSULFATES WITH N-NUCLEOPHILES". . p. 435 - 438. Retrieved 2007/10/02.