(m-HC₆Cl₄)2Hg

Base Information

• Chemical Name: (m-HC₆Cl₄)2Hg
• CAS No.: 37963-59-0
• Molecular Formula: C₁₂H₂Cl₈Hg
• Molecular Weight: 630.362
• Mol file: 37963-59-0.mol

Synonyms:(m-HC₆Cl₄)2Hg

Chemical Property of (m-HC₆Cl₄)2Hg

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of (m-HC₆Cl₄)2Hg

There total 1 articles about (m-HC₆Cl₄)2Hg which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

Hg(O3S-m-HC6Cl4)2*2H2O → (m-HC6Cl4)2Hg (37963-59-0) + sulfur trioxide (7446-11-9)

Guidance literature:

130-220°C;

Reference yield: 95.0%

(m-HC6Cl4)2Hg (37963-59-0) + mercury dichloride → ClHg(2,3,4,6-C6HCl4) (84015-03-2)

Guidance literature:

In xylene; refluxed for 2 h; recrystd. twice from dichloromethane-methanol; elem. anal.;

DOI:10.1016/S0277-5387(00)87159-4

Reference yield: 60.0%

cis-dichlorobis(triphenylphosphine)platinum(II) (10199-34-5,14056-88-3,15604-36-1) + (m-HC6Cl4)2Hg (37963-59-0) → PtCl(C6HCl4)(P(C6H5)3)2 (77321-86-9)

Guidance literature:

In neat (no solvent); byproducts: Hg(2,3,4,6-C6HCl4)Cl; a mixt. of Pt-complex and Hg-compound was heated at 290°C for 5 min, cooled to room temp.; extd. with CH2Cl2, MeOH was added, Hg-compound was removed by vac. sublimation (130°C; 0.05 mmHg); elem. anal.;

DOI:10.1016/S0022-328X(00)82944-7

Downstream raw materials:

ClHg(2,3,4,6-C₆HCl₄)

PtCl(C₆HCl₄)(P(C₆H₅)3)2