Vat Green 1

Base Information

• Chemical Name: Vat Green 1
• CAS No.: 128-58-5
• Deprecated CAS: 12663-53-5,12797-84-1,37338-82-2,52415-15-3,57107-67-2,57455-89-7,61356-60-3,113255-70-2,625849-96-9,12797-84-1,37338-82-2,52415-15-3,57107-67-2,57455-89-7,61356-60-3,625849-96-9
• Molecular Formula: C36H20O4
• Molecular Weight: 516.552
• Hs Code.: 2914509090
• European Community (EC) Number: 204-896-6,814-890-0,841-225-1
• UNII: 5C13513T4R
• DSSTox Substance ID: DTXSID4044531
• Nikkaji Number: J5.408I
• Wikipedia: Vat_Green_1
• Wikidata: Q17047307
• Mol file: 128-58-5.mol

Synonyms:Vat Green 1;128-58-5;16,17-Dimethoxyanthra[9,1,2-cde]benzo[rst]pentaphene-5,10-dione;C.I. Vat Green 1;CI VAT GREEN 1;Caledon Jade Green;Vat Brilliant Green C;Jade Green Base;Brilliant Green S;Mayvat Jade Green;Dimethoxyviolanthrone;Helanthrene Green B;Amanthrene Green JF;Indanthren Brilliant Green B;Palanthrene Jade Green Supra;16,17-Dimethoxyviolanthrone;Mikethrene Green FFB;Ostanthren Green FFB;Ahcovat Jade Green B;Navinon Jade Green B;Belanthrene Jade Green;Palanthrene Jade Green;Caledon Jade Green XN;Paradone Jade Green B;Vat Brilliant Green S;Benzadone Jade Green B;Benzadone Jade Green X;Calcoloid Jade Green N;Brilliant Green Anthraquinone S;Paradone Jade Green BX;Paradone Jade Green XS;Ahcovat Jade Green BDA;Caledon Jade Green XBN;Navinon Jade Green FFB;Benzadone Jade Green XN;Calcoloid Jade Green NC;Calcoloid Jade Green NP;Tinon Brilliant Green BF;Violanthrone, 16,17-dimethoxy-;Zelen kypova 1 [Czech];Atic Vat Jade Green XBN;Benzadone Jade Green XBN;Amanthrene Supra Green JF;Tinon Brilliant Green BFP;Zelen kypova 1;Tinon Brilliant Green 2BF;Carbanthrene Brilliant Green;Tyrian Brilliant Green I-B;Amanthrene Brilliant Green J;Fenanthren Brilliant Green B;Mikethrene Brilliant Green B;Nyanthrene Brilliant Green B;Cibanone Brilliant Green 2BF;Cibanone Brilliant Green FBF;Indanthrene Brilliant Green B;Nihonthrene Brilliant Green B;Solanthrene Brilliant Green B;Amanthrene Brilliant Green JP;Indanthren Brilliant Green FB;Romantrene Brilliant Green FB;Tinon Brilliant Green B2F-F;Tyrian Brilliant Green I-FFB;Ahcovat Printing Jade Green B;Carbanthrene Brilliant Green G;Indanthrene Brilliant Green BN;Pernithrene Brilliant Green GG;Solanthrene Brilliant Green BN;Solanthrene Brilliant Green FF;Indanthren Brilliant Green FFB;Mikethrene Brilliant Green FFB;Ostanthren Brilliant Green FFB;Romantrene Brilliant Green FFB;Caledon Printing Jade Green XN;Indanthrene Brilliant Green FFB;Nihonthrene Brilliant Green FFB;Parnithrene Brilliant Green FFB;Sandothrene Brilliant Green NBF;16,17-Dimethoxyviolanthrene-5,10-dione;CI 59825;Ahcovat Printing Jade Green BDA;Caledon Printing Jade Green XBN;HSDB 5474;Atic Vat Printing Jade Green XBN;EINECS 204-896-6;BRN 2068558;Indanthren Brilliant Green FFB Extra Pure;Zelen Ostanthrenova Brilantni FFB [Czech];Paradone Jade Green B new, BX new XS new;C.I. 59825;UNII-5C13513T4R;Zelen Ostanthrenova Brilantni FFB;5C13513T4R;Anthra(9,1,2-cde)benzo(rst)pentaphene-5,10-dione, 16,17-dimethoxy-;Dinaphtho(1,2,3-cd:3',2',1'-lm)perylene-5,10-dione, 16,17-dimethoxy-;16,17-Dimethoxyanthra[9,1,2-cde]-benzo[rst]pentaphene-5,10-dione;Anthra[9,1,2-cde]benzo[rst]pentaphene-5,10-dione, 16,17-dimethoxy-;Dinaphtho[1,2,3-cd:3',2',1'-lm]perylene-5,10-dione, 16,17-dimethoxy-;Vat Green1;C.I.Vat Green 1;Color Index No. 59825;Color Index Number 59825;Colour Index No. 59825;Colour Index Number 59825;SCHEMBL3408840;DTXSID4044531;AKOS003617689;C.I. 59825 [HSDB];LS-62046;A907914;Q17047307;ANTHRA(9,1,2-CDE)BENZO(RST)PENTAPHENE-5,10-DIONE, 16,17- DIMETHOXY-;C.I. Vat green 1: 16,17-Dimethoxydinaphtho (1,2,3-cd:3',2',1'-lm) perylene-5,10-dione;DINAPHTHO(1,2,3-CD:3',2',1'-LM)PERYLENE-5,10-DIONE, 16,17- DIMETHOXY-;30,34-dimethoxynonacyclo[18.10.2.2^{2,5.0^{3,16.0^{4,13.0^{6,11.0^{17,31.0^{22,27.0^{28,32]tetratriaconta-1(30),2(34),3(16),4(13),5(33),6,8,10,14,17(31),18,20(32),22,24,26,28-hexadecaene-12,21-dione;30,34-dimethoxynonacyclo[18.10.2.22,5.03,16.04,13.06,11.017,31.022,27.028,32]tetratriaconta-1(30),2(34),3(16),4(13),5(33),6,8,10,14,17(31),18,20(32),22,24,26,28-hexadecaene-12,21-dione

Chemical Property of Vat Green 1

Chemical Property:

• Appearance/Colour: solid
• Refractive Index: 1.799
• Boiling Point: 521.39°C (rough estimate)
• PSA: 52.60000
• Density: 1.455 g/cm³
• LogP: 8.17720
• XLogP3: 8
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 2
• Exact Mass: 516.13615911
• Heavy Atom Count: 40
• Complexity: 971

Purity/Quality:

99.9% ^*data from raw suppliers

16,17-Dimethoxyanthra[9,1,2-cde]-benzo[rst]pentaphene-5,10-dione 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Chemical Classes: Dyes -> Other Dyes
• Canonical SMILES: COC1=C2C3=C(C=CC4=C3C(=C1)C5=CC=CC=C5C4=O)C6=C7C2=C(C=C8C7=C(C=C6)C(=O)C9=CC=CC=C98)OC
• Uses: 16,17-Dimethoxyanthra[9,1,2-cde]-benzo[rst]pentaphene-5,10-dione is used in producing colored fibrous materials.

Technology Process of Vat Green 1

There total 8 articles about Vat Green 1 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-methoxy-benz[de]anthracen-7-one (6535-67-7) → Jade Green XBN (128-58-5)

Guidance literature:

With potassium hydroxide; ethanol; at 130 - 140 ℃; Behandeln des Reaktionsprodukts mit Luft;

Reference yield:

isoviolanthrone (116-71-2) + methyl p-toluene sulfonate (80-48-8) → Jade Green XBN (128-58-5)

Guidance literature:

With tetralin; sodium carbonate; auf Siedetemperatur;

Reference yield:

isoviolanthrone (116-71-2) + dimethyl sulfate (77-78-1) → Jade Green XBN (128-58-5)

Guidance literature:

With potassium carbonate; 1,2,3-trichlorobenzene; unter Zusatz von Phenol, Naphthol-⁽¹⁾ oder Hydrochinon auf 180grad;

upstream raw materials:

2-methoxy-benz[de]anthracen-7-one

isoviolanthrone

methyl p-toluene sulfonate

dimethyl sulfate

Downstream raw materials:

16,17-bis(octyloxy)-anthra[9,1,2-cde-]benzo[rst]pentaphene-5,10-dione

16,17-didecyloxyviolanthrone

16,17-dihydroxyviolanthrene-5,10-dione

16,17-dimethoxy-5,10-bis-sulfooxy-anthra[9,1,2-cde]benzo[rst]pentaphene