Zr(CH₂C(CH₃)3)2Br₂(CH₃CH₂OCH₂CH₃)2

Base Information

• Chemical Name: Zr(CH₂C(CH₃)3)2Br₂(CH₃CH₂OCH₂CH₃)2
• CAS No.: 78068-03-8
• Molecular Formula: C₁₈H₄₂Br₂O₂Zr
• Molecular Weight: 541.562
• Mol file: 78068-03-8.mol

Synonyms:Zr(CH₂C(CH₃)3)2Br₂(CH₃CH₂OCH₂CH₃)2

Chemical Property of Zr(CH₂C(CH₃)3)2Br₂(CH₃CH₂OCH₂CH₃)2

Chemical Property:

Purity/Quality:

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Technology Process of Zr(CH₂C(CH₃)3)2Br₂(CH₃CH₂OCH₂CH₃)2

There total 1 articles about Zr(CH₂C(CH₃)3)2Br₂(CH₃CH₂OCH₂CH₃)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

diethyl ether (60-29-7,927820-24-4) + zirconium(IV) bromide (13777-25-8) + neopentyl lithium (7412-67-1) → Zr(CH2C(CH3)3)2Br2(CH3CH2OCH2CH3)2 (78068-03-8)

Guidance literature:

In diethyl ether; byproducts: LiCl; soln. of LiCH2C(CH3)3 added to suspn. of ZrCl4 dropwise over 1 h at room temp., stirred for 15 min, under N2, light excluded; filtered. evapd. in vac., extd. with pentane-ether, filtered, evapd. invac.;

DOI:10.1016/S0022-328X(00)82434-1

upstream raw materials:

diethyl ether

zirconium(IV) bromide

neopentyl lithium

Refernces