Technology Process of C30H33BrN2O5S
There total 11 articles about C30H33BrN2O5S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
di-isopropyl azodicarboxylate; triphenylphosphine;
In
tetrahydrofuran;
at 20 ℃;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: sodium hydride / 1,4-dioxane / 0.25 h / 10 °C
1.2: 10 - 100 °C
2.1: sodium hydroxide; water / methanol / 4 h / 50 °C
3.1: potassium carbonate; silver(I) acetate; 1-methyl-pyrrolidin-2-one / 2 h / 110 °C
4.1: bromine; CH3COONa / acetic acid / 1 h / 20 °C
5.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 20 °C / Inert atmosphere
With
1-methyl-pyrrolidin-2-one; di-isopropyl azodicarboxylate; CH3COONa; water; bromine; silver(I) acetate; sodium hydride; potassium carbonate; triphenylphosphine; sodium hydroxide;
In
tetrahydrofuran; 1,4-dioxane; methanol; acetic acid;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: sodium hydride / 1,4-dioxane / 0.25 h / 10 °C
1.2: 10 - 100 °C
2.1: sodium hydroxide; water / methanol / 4 h / 50 °C
3.1: potassium carbonate; silver(I) acetate; 1-methyl-pyrrolidin-2-one / 2 h / 110 °C
4.1: bromine; CH3COONa / acetic acid / 1 h / 20 °C
5.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 20 °C / Inert atmosphere
With
1-methyl-pyrrolidin-2-one; di-isopropyl azodicarboxylate; CH3COONa; water; bromine; silver(I) acetate; sodium hydride; potassium carbonate; triphenylphosphine; sodium hydroxide;
In
tetrahydrofuran; 1,4-dioxane; methanol; acetic acid;