Methyl 6-chloro-2,4,4-trimethyl-4H-1,3-benzodioxin-2-carboxylate

Base Information Edit

Chemical Name:Methyl 6-chloro-2,4,4-trimethyl-4H-1,3-benzodioxin-2-carboxylate
CAS No.:73050-94-9
Molecular Formula:C₁₃H₁₅ClO₄
Molecular Weight:270.713
Hs Code.:
DSSTox Substance ID:DTXSID00993822
Mol file:73050-94-9.mol

Synonyms:BRN 5064102;73050-94-9;Methyl 6-chloro-2,4,4-trimethyl-4H-1,3-benzodioxin-2-carboxylate;1,3-Benzodioxan-2-carboxylic acid, 6-chloro-2,4,4-trimethyl-, methyl ester;4H-1,3-Benzodioxin-2-carboxylic acid, 6-chloro-2,4,4-trimethyl-, methyl ester;6-Chloro-2,4,4-trimethyl (4H) 1,3-benzodioxin-2-carboxylate de methyle [French];C13H15ClO4;6-Chloro-2,4,4-trimethyl (4H) 1,3-benzodioxin-2-carboxylate de methyle;SCHEMBL11368270;DTXSID00993822;LS-34564;Methyl 6-chloro-2,4,4-trimethyl-2H,4H-1,3-benzodioxine-2-carboxylate

Suppliers and Price of Methyl 6-chloro-2,4,4-trimethyl-4H-1,3-benzodioxin-2-carboxylate

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Methyl 6-chloro-2,4,4-trimethyl-4H-1,3-benzodioxin-2-carboxylate Edit

Chemical Property:

Vapor Pressure:1.87E-05mmHg at 25°C
Boiling Point:362.9°C at 760 mmHg
Flash Point:143.7°C
Density:1.204g/cm³
XLogP3:2.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:270.0658866
Heavy Atom Count:18
Complexity:344

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1(C2=C(C=CC(=C2)Cl)OC(O1)(C)C(=O)OC)C

Technology Process of Methyl 6-chloro-2,4,4-trimethyl-4H-1,3-benzodioxin-2-carboxylate

There total 2 articles about Methyl 6-chloro-2,4,4-trimethyl-4H-1,3-benzodioxin-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 73050-78-9
2-(5-chloro-2-hydroxy-phenyl)-propan-2-ol

: 73050-94-9
6-Chloro-2,4,4-trimethyl-4H-benzo[1,3]dioxine-2-carboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 50percent NaH/mineral oil, 18 crown 6 / dioxane / 3 h / 65 °C

2: Redex CF resin

With 18-crown-6 ether; Redex CF resin; sodium hydride; mineral oil; In 1,4-dioxane;