Methyltributylammonium iodide

Base Information

• Chemical Name: Methyltributylammonium iodide
• CAS No.: 3085-79-8
• Molecular Formula: C13H30 N . I
• Molecular Weight: 327.292
• Hs Code.: 2923900090
• European Community (EC) Number: 221-402-4
• NSC Number: 136982
• DSSTox Substance ID: DTXSID8091534
• Mol file: 3085-79-8.mol

Synonyms:TBuMA;tri-n-butylmethylammonium;tri-n-butylmethylammonium chloride;tri-n-butylmethylammonium hydroxide;tri-n-butylmethylammonium sulfate (1:1);tributylmethylammonium;tributylmethylammonium iodide

Chemical Property of Methyltributylammonium iodide

Chemical Property:

• Melting Point: 184-185 °C
• Boiling Point: °Cat760mmHg
• Flash Point: °C
• PSA: 0.00000
• Density: g/cm³
• LogP: 0.83730
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 9
• Exact Mass: 327.14230
• Heavy Atom Count: 15
• Complexity: 98.6

Purity/Quality:

99% ^*data from raw suppliers

Tributylmethylammonium Iodide >98.0%(T) ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26-36

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

• Canonical SMILES: CCCC[N+](C)(CCCC)CCCC.[I-]

Technology Process of Methyltributylammonium iodide

There total 2 articles about Methyltributylammonium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

tributyl-amine (102-82-9) + methyl iodide (74-88-4) → tri(n-butyl)methylammonium iodide (3085-79-8)

Guidance literature:

In butanone; at 20 ℃; for 5h; Heating;

DOI:10.1016/S0022-2860(00)00774-2

Reference yield:

→ tri(n-butyl)methylammonium iodide (3085-79-8)

Guidance literature:

Tributylamin, Methyliodid, Acetonitril;

Reference yield:

tri(n-butyl)methylammonium iodide (3085-79-8) + ammonia (7664-41-7) → 1-butylene (106-98-9,9003-28-5) + tributyl-amine (102-82-9) + methane (34557-54-5,27936-85-2) + N-methyldibutylamine (3405-45-6)

Guidance literature:

DOI:10.1021/ja01527a023 DOI:10.1021/ja01527a024

upstream raw materials:

tributyl-amine

methyl iodide

Downstream raw materials:

1-butylene

tributyl-amine

methane

N-methyldibutylamine

Refernces

• 1、 Nevecna, Tat'jana,Bekarek, Vojtech. "SIGNIFICANCE TEST OF REFRACTIVE INDEX OF SOLVENT IN EVALUATION OF EFFECT OF MEDIUM ON RATES OF QUATERNIZATION REACTIONS OF METHYL IODIDE WITH AMINES". . p. 180 - 184. Retrieved 2007/10/02.