Diazodinitrophenol

Base Information

• Chemical Name: Diazodinitrophenol
• CAS No.: 4682-03-5
• Molecular Formula: C6H2N4O5
• Molecular Weight: 210.106
• Mol file: 4682-03-5.mol

Synonyms:3.5-Dinitro-benzochinon-(1.2)-diazid-(1);2-hydroxy-3,5-dinitro-benzenediazonium-betaine;2-Hydroxy-3,5-dinitro-benzoldiazonium-betain;1.3-Dinitro-5-diazo-cyclohexadien-(1.3)-on-(6);3.5-Dinitro-o-chinon-diazid-(1);6-diaza-2,4-dinitrophenolate;

Chemical Property of Diazodinitrophenol

Chemical Property:

• Refractive Index: 1.6900 (estimate)
• Boiling Point: °Cat760mmHg
• Flash Point: °C
• PSA: 142.85000
• Density: g/cm³
• LogP: 3.17778

Purity/Quality:

99.9% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

Technology Process of Diazodinitrophenol

There total 10 articles about Diazodinitrophenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

2-chloro-3,5-dinitroaniline (88140-44-7) → 2-hydroxy-3,5-dinitro-benzenediazonium betaine (4682-03-5)

Guidance literature:

With nitric acid; In various solvent(s); Ambient temperature;

DOI:10.1021/jo00363a032

Reference yield:

N,2,3,5-tetranitroaniline (57204-57-6) → 2-hydroxy-3,5-dinitro-benzenediazonium betaine (4682-03-5)

Guidance literature:

In ethyl acetate; at 60 ℃;

DOI:10.1021/jo00363a032

Reference yield:

2-chloro-3,5-dinitrobenzoic acid (2497-91-8) → 2-hydroxy-3,5-dinitro-benzenediazonium betaine (4682-03-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 20percent oleum, sodium azide / 1,2-dichloro-ethane / 3 h / Heating

2: 36 percent / 100percent nitric acid / various solvent(s) / Ambient temperature

With sodium azide; sulfuric acid; nitric acid; In 1,2-dichloro-ethane;

DOI:10.1021/jo00363a032

upstream raw materials:

picramic acid

N,2,3,5-tetranitroaniline

2-chloro-3,5-dinitroaniline

sodium picramate

Downstream raw materials:

3,5-dinitro-[1,2]benzoquinone-1-(triphenylphosphoranylidene-hydrazone)

2,4-Dinitrophenol

2-(2-Hydroxy-3,5-dinitrophenyl-hydrazono)-3-oxo-buttersaeureaethylester

Refernces

• 1、 Mudge et al.. "". . p. 569. Retrieved 1975.
• 2、 Spear, Robert J.,Elischer, Paul P.. "Studies of Stab Initiation. Sensitization of Lead Azide by Energetic Sensitizers". . p. 1 - 13. Retrieved 2007/10/02.