benzoic hydrazide hydrochloride

Base Information

• Chemical Name: benzoic hydrazide hydrochloride
• CAS No.: 1452-58-0
• Molecular Formula: C₇H₉N₂O*Cl
• Molecular Weight: 172.614
• Mol file: 1452-58-0.mol

Synonyms:benzoic hydrazide hydrochloride

Chemical Property of benzoic hydrazide hydrochloride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of benzoic hydrazide hydrochloride

There total 5 articles about benzoic hydrazide hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

2,5,7-Triphenyl-7,7a,8,9,10,11-hexahydro[1,3,4]oxadiazolo[2,3-j]quinoline (70194-72-8) → benzoic hydrazide hydrochloride (1452-58-0) + 2-(3-oxo-1,3-diphenylpropyl)cyclohexanone (2682-98-6)

Guidance literature:

With hydrogenchloride; In benzene;

Reference yield:

N'-benzoylhydrazinecarboxylic acid tert-butyl ester (92789-04-3) → benzoic hydrazide hydrochloride (1452-58-0)

Guidance literature:

With hydrogenchloride; In methanol; at 0 ℃; for 1h;

DOI:10.3390/molecules24244440

Reference yield:

benzoyl chloride (98-88-4) → benzoic hydrazide hydrochloride (1452-58-0)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine / dichloromethane / 5 h / 20 °C

2: hydrogenchloride / methanol / 1 h / 0 °C

With pyridine; hydrogenchloride; In methanol; dichloromethane;

DOI:10.3390/molecules24244440

upstream raw materials:

2,5,7-Triphenyl-7,7a,8,9,10,11-hexahydro[1,3,4]oxadiazolo[2,3-j]quinoline

hydrogenchloride

chloroform

α,α-azodioxytoluene

Downstream raw materials:

[1,2]naphthoquinone-2-benzoylhydrazone

Benzoic acid N'-[2-chloro-2-(4-chloro-phenyl)-acetyl]-hydrazide

Benzoic acid N'-[2-chloro-2-(4-nitro-phenyl)-acetyl]-hydrazide

C₁₆H₁₁N₃O

Refernces

• 1、 Moskovkina. "Some reactions of hexahydro[1,3,4]oxadiazolo2,3-j|quinolines and pathways of their formation". . p. 1077 - 1081. Retrieved 2007/10/03.