Benzenecarboximidic acid methyl ester

Base Information

• Chemical Name: Benzenecarboximidic acid methyl ester
• CAS No.: 7471-86-5
• Molecular Formula: C8H9NO
• Molecular Weight: 135.166
• Mol file: 7471-86-5.mol

Synonyms:Benzimidicacid, methyl ester (6CI,7CI,8CI);Methyl benzimidate;NSC 402222;

Chemical Property of Benzenecarboximidic acid methyl ester

Chemical Property:

• Vapor Pressure: 1.89mmHg at 25°C
• Refractive Index: 1.503
• Boiling Point: 171.1 °C at 760 mmHg
• Flash Point: 57.3 °C
• PSA: 33.08000
• Density: 1 g/cm³
• LogP: 1.75810

Purity/Quality:

99.5% ^*data from raw suppliers

BenzenecarboximidicAcidMethylEster ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzenecarboximidic acid methyl ester

There total 14 articles about Benzenecarboximidic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

→ methyl benzimidate (7471-86-5)

Guidance literature:

Reference yield:

methyl N-(phenyldichloroseleno)benzimidate (78488-67-2) → benzeneseleninic acid (6996-92-5) + methyl benzimidate (7471-86-5)

Guidance literature:

With sodium hydroxide; In diethyl ether; at 20 ℃; for 1h; Yield given. Yields of byproduct given;

Reference yield:

C14H14N2OSe → diphenyl diselenide (1666-13-3) + methyl benzimidate (7471-86-5)

Guidance literature:

upstream raw materials:

diethyl ether

benzamide; silver-salt

methyl iodide

benzamide

Downstream raw materials:

N-(Methoxyphenylmethylen)carbamidsaeure-ethylester

2-Phenylimidazole

2-phenyl-1H-benzoimidazole

N-methyl-2-phenyl-1H-imidazole

Refernces

• 1、 Oh, Sangmi,Libardo, M. Daben J.,Azeeza, Shaik,Pauly, Gary T.,Roma, Jose Santinni O.,Sajid, Andaleeb,Tateishi, Yoshitaka,Duncombe, Caroline,Goodwin, Michael,Ioerger, Thomas R.,Wyatt, Paul G.,Ray, Peter C.,Gray, David W.,Boshoff, Helena I. M.,Barry, Clifton E.. "Structure-Activity Relationships of Pyrazolo[1,5- a]pyrimidin-7(4 H)-ones as Antitubercular Agents". . p. 479 - 492. Retrieved 2021/01/26.
• 2、 Moiola, Mattia,Leusciatti, Marco,Quadrelli, Paolo. "Reactions of 1,2,4-Oxadiazole[4,5-a]piridinium Salts with Alcohols: the Synthesis of Alkoxybutadienyl 1,2,4-Oxadiazoles". . p. 195 - 199. Retrieved 2020/03/06.