Disodium;5-[(4,6-dianilino-1,3,5-triazin-2-yl)amino]-2-[2-[4-[(4,6-dianilino-1,3,5-triazin-2-yl)amino]-2-sulfonatophenyl]ethenyl]benzenesulfonate

Base Information

• Chemical Name: Disodium;5-[(4,6-dianilino-1,3,5-triazin-2-yl)amino]-2-[2-[4-[(4,6-dianilino-1,3,5-triazin-2-yl)amino]-2-sulfonatophenyl]ethenyl]benzenesulfonate
• CAS No.: 133-66-4
• Deprecated CAS: 122414-16-8,61550-54-7,878766-85-9
• Molecular Formula: C44H36 N12 O6 S2 . 2 Na
• Molecular Weight: 936.942
• European Community (EC) Number: 205-117-2
• DSSTox Substance ID: DTXSID90889422
• Mol file: 133-66-4.mol

Synonyms:cellu-brite

Chemical Property of Disodium;5-[(4,6-dianilino-1,3,5-triazin-2-yl)amino]-2-[2-[4-[(4,6-dianilino-1,3,5-triazin-2-yl)amino]-2-sulfonatophenyl]ethenyl]benzenesulfonate

Chemical Property:

• Boiling Point: °Cat760mmHg
• PKA: -1.05[at 20 ℃]
• Flash Point: °C
• PSA: 280.68000
• Density: g/cm³
• LogP: 11.09640
• Water Solubility.: 140mg/L at 20℃
• Hydrogen Bond Donor Count: 6
• Hydrogen Bond Acceptor Count: 18
• Rotatable Bond Count: 14
• Exact Mass: 936.19610776
• Heavy Atom Count: 66
• Complexity: 1460

Purity/Quality:

99.9% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)NC2=NC(=NC(=N2)NC3=CC(=C(C=C3)C=CC4=C(C=C(C=C4)NC5=NC(=NC(=N5)NC6=CC=CC=C6)NC7=CC=CC=C7)S(=O)(=O)[O-])S(=O)(=O)[O-])NC8=CC=CC=C8.[Na+].[Na+]

Technology Process of Disodium;5-[(4,6-dianilino-1,3,5-triazin-2-yl)amino]-2-[2-[4-[(4,6-dianilino-1,3,5-triazin-2-yl)amino]-2-sulfonatophenyl]ethenyl]benzenesulfonate

There total 2 articles about Disodium;5-[(4,6-dianilino-1,3,5-triazin-2-yl)amino]-2-[2-[4-[(4,6-dianilino-1,3,5-triazin-2-yl)amino]-2-sulfonatophenyl]ethenyl]benzenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 23.4%

6,6'-(ethene-1,2-diyl)bis(3-((4-chloro-6-(phenylamino)-1,3,5-triazin-2-yl)amino)benzenesulfonic acid)disodium salt + aniline (62-53-3) → disodium 4,4'-bis[(4,6-dianilino-1,3,5-triazin-2-yl)amino]stilbene-2,2'-disulphonate (133-66-4)

Guidance literature:

6,6'-(ethene-1,2-diyl)bis(3-((4-chloro-6-(phenylamino)-1,3,5-triazin-2-yl)amino)benzenesulfonic acid)disodium salt; aniline; In polyethyleneglycol-300; at 130 ℃; for 0.5h;

With sodium hydroxide; In water;

Reference yield:

→ disodium 4,4'-bis[(4,6-dianilino-1,3,5-triazin-2-yl)amino]stilbene-2,2'-disulphonate (133-66-4)

Guidance literature:

from trichloro-s-triazine and corresponding bases;

upstream raw materials:

aniline

Refernces

• 1、 -. "Process for the preparation of stilbene compounds". Example 2. . Retrieved 2008/06/13.