3'-(α-Brompropionyl)-methansulfonanilid

Base Information

• Chemical Name: 3'-(α-Brompropionyl)-methansulfonanilid
• CAS No.: 5317-86-2
• Molecular Formula: C₁₀H₁₂BrNO₃S
• Molecular Weight: 306.18
• Mol file: 5317-86-2.mol

Synonyms:3'-(α-Brompropionyl)-methansulfonanilid

Chemical Property of 3'-(α-Brompropionyl)-methansulfonanilid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3'-(α-Brompropionyl)-methansulfonanilid

There total 4 articles about 3'-(α-Brompropionyl)-methansulfonanilid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3'-nitropropiophenone (17408-16-1) → 3'-(α-Brompropionyl)-methansulfonanilid (5317-86-2)

Guidance literature:

Multi-step reaction with 3 steps

1: H₂ / PtO₂ / methanol

2: Py

3: Br₂, (PhCO)2O₂ / diethyl ether

With pyridine; hydrogen; bromine; dibenzoyl peroxide; platinum(IV) oxide; In methanol; diethyl ether;

DOI:10.1021/jm00319a023

Reference yield:

N-methanesulfonyl-3-aminopropiophenone (5317-85-1) → 3'-(α-Brompropionyl)-methansulfonanilid (5317-86-2)

Guidance literature:

With bromine; dibenzoyl peroxide; In diethyl ether;

DOI:10.1021/jm00319a023

Reference yield:

1-(3-amino-phenyl)-propan-1-one (1197-05-3) → 3'-(α-Brompropionyl)-methansulfonanilid (5317-86-2)

Guidance literature:

Multi-step reaction with 2 steps

1: Py

2: Br₂, (PhCO)2O₂ / diethyl ether

With pyridine; bromine; dibenzoyl peroxide; In diethyl ether;

DOI:10.1021/jm00319a023

upstream raw materials:

N-methanesulfonyl-3-aminopropiophenone

3'-nitropropiophenone

1-(3-amino-phenyl)-propan-1-one

Refernces

• 1、 Uloth,Kirk,Gould,Larsen. "Sulfonanilides. I. Monoalkyl- and arylsulfonamidophenethanolamines.". . p. 88 - 97. Retrieved 2007/10/05.