Technology Process of Dimethyl methylphosphonite
There total 7 articles about Dimethyl methylphosphonite which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tri-n-propylamine;
In
Petroleum ether;
at 25 - 60 ℃;
for 1.5h;
Time;
Flow reactor;
Large scale;
- Guidance literature:
-
With
phenylsilane;
at 5 - 90 ℃;
for 1h;
Inert atmosphere;
- Guidance literature:
-
methylene chloride;
With
magnesium;
In
tetrahydrofuran; 5,5-dimethyl-1,3-cyclohexadiene;
at 50 ℃;
for 3h;
dimethyl chlorophosphite;
In
tetrahydrofuran; 5,5-dimethyl-1,3-cyclohexadiene;
at 15 - 30 ℃;
for 6h;
