Fluoridophosphoric acid dicyclohexyl ester

Base Information

• Chemical Name: Fluoridophosphoric acid dicyclohexyl ester
• CAS No.: 587-15-5
• Molecular Formula: C12H22FO3P
• Molecular Weight: 264.277
• Mol file: 587-15-5.mol

Synonyms:fluorophosphoric acid dicyclohexyl ester;Phosphorofluoridic acid,dicyclohexyl ester;Cyclohexyl phsophorofluoridate;Dicyclohexyl fluorophosphonate;Phosphorsaeure-dicyclohexylester-fluorid;Fluorophosphorsaeure-dicyclohexylester;dicyclohexyl phosphorofluoridate;Dicyclohexyl-fluorphosphat;

Chemical Property of Fluoridophosphoric acid dicyclohexyl ester

Chemical Property:

• Vapor Pressure: 0.00027mmHg at 25°C
• Boiling Point: 333.1°C at 760 mmHg
• Flash Point: 155.3°C
• PSA: 45.34000
• Density: 1.12g/cm³
• LogP: 4.76260

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Fluoridophosphoric acid dicyclohexyl ester

There total 3 articles about Fluoridophosphoric acid dicyclohexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

dicyclohexyl phosphonate (3808-22-8) → dicyclohexyl phosphorofluoridate (587-15-5)

Guidance literature:

With potassium fluoride; trichloroacetonitrile; for 0.583333h; Heating;

DOI:10.1016/j.tetlet.2008.02.051

Reference yield:

dicyclohexyl phosphorochloridate (51672-37-8) → dicyclohexyl phosphorofluoridate (587-15-5)

Guidance literature:

With ammonium fluoride; acetone;

Reference yield:

cyclohexanol (108-93-0) → dicyclohexyl phosphorofluoridate (587-15-5)

Guidance literature:

With phosphoryl dichloride fluoride; diethyl ether; unter Durchleiten von trockener Luft und anschliessende Behandlung mit NH₃;

DOI:10.1039/jr9480001010

upstream raw materials:

dicyclohexyl phosphorochloridate

cyclohexanol

dicyclohexyl phosphonate

Refernces

• 1、 Gupta,Acharya,Pardasani,Dubey. "Single step fluorination of dialkylphosphites: trichloroacetonitrile-KF as an efficient reagent for the synthesis of dialkyl fluorophosphates". . p. 2232 - 2235. Retrieved 2008/09/19.