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dimethyl N-benzylphosphoramidothionate

Base Information Edit
  • Chemical Name:dimethyl N-benzylphosphoramidothionate
  • CAS No.:130012-35-0
  • Molecular Formula:C9H14NO2PS
  • Molecular Weight:231.255
  • Hs Code.:
  • Mol file:130012-35-0.mol
dimethyl N-benzylphosphoramidothionate

Synonyms:dimethyl N-benzylphosphoramidothionate

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Chemical Property of dimethyl N-benzylphosphoramidothionate Edit
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Technology Process of dimethyl N-benzylphosphoramidothionate

There total 1 articles about dimethyl N-benzylphosphoramidothionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With triethylamine; In dichloromethane; for 20h; Ambient temperature;
DOI:10.1021/jo00312a012
Guidance literature:
With monoperoxyphthalic acid; magnesium salt; In dichloromethane; for 12h; Heating;
DOI:10.1016/S0040-4039(00)60006-0
Guidance literature:
Multi-step reaction with 3 steps
1: 1.) sodium hydride / 1.) THF, reflux, 2 h, 2.) 0 deg C to room temperature, 15-30 min.
2: CCl4 / Heating
3: 1 M aq. HCl / tetrahydrofuran / Ambient temperature
With hydrogenchloride; sodium hydride; In tetrahydrofuran; tetrachloromethane;
DOI:10.1021/jo00312a012
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