ALLYLCYCLOHEXANE ACETATE

Base Information

• Chemical Name: ALLYLCYCLOHEXANE ACETATE
• CAS No.: 4728-82-9
• Molecular Formula: C11H18 O2
• Molecular Weight: 182.263
• Mol file: 4728-82-9.mol

Synonyms:Cyclohexaneaceticacid, 2-propenyl ester (9CI); Cyclohexaneacetic acid, allyl ester (7CI,8CI);Allyl cyclohexaneacetate; Allyl cyclohexylacetate

Chemical Property of ALLYLCYCLOHEXANE ACETATE

Chemical Property:

• Vapor Pressure: 0.027mmHg at 25°C
• Refractive Index: 1.4614 (estimate)
• Boiling Point: 246.7°Cat760mmHg
• Flash Point: 98.8°C
• PSA: 26.30000
• Density: 0.948g/cm³
• LogP: 2.68600

Purity/Quality:

99% ^*data from raw suppliers

ALLYLCYCLOHEXANE ACETATE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Description: A liquid with an intense, sweet, long-lasting fruital (pineapple, peach, apricot) aroma. It is used as a flavor enhancer, flavoring agent and adjuvant.

Technology Process of ALLYLCYCLOHEXANE ACETATE

There total 2 articles about ALLYLCYCLOHEXANE ACETATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Cyclohexylacetic acid (5292-21-7) + allyl alcohol (107-18-6) → cyclohexyl-acetic acid allyl ester (4728-82-9)

Guidance literature:

Cyclohexylacetic acid; With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 25 ℃; for 0.166667h;

allyl alcohol; In dichloromethane; at 25 ℃; for 1h;

DOI:10.1021/jacs.8b05560

Reference yield:

allyl diazoacetate (4606-10-4) + cyclohexane (110-82-7,25012-93-5) → cyclohexyl-acetic acid allyl ester (4728-82-9)

Guidance literature:

Irradiation;

Reference yield:

cyclohexyl-acetic acid allyl ester (4728-82-9) + benzoyl chloride (98-88-4) → allyl 2-cyclohexyl-3-oxo-3-phenylpropanoate

Guidance literature:

With 1-methyl-1H-imidazole; titanium tetrachloride; triethylamine; In dichloromethane; at -45 ℃; for 2.33333h;

DOI:10.1021/jacs.8b05560

upstream raw materials:

allyl diazoacetate

cyclohexane

Cyclohexylacetic acid

allyl alcohol

Refernces