Benzaldehyde,4-(1H-pyrrol-1-yl)-

Base Information

• Chemical Name: Benzaldehyde,4-(1H-pyrrol-1-yl)-
• CAS No.: 23351-05-5
• Molecular Formula: C11H9NO
• Molecular Weight: 171.199
• Hs Code.: 2933990090
• Mol file: 23351-05-5.mol

Synonyms:4-Pyrrol-1-yl-benzaldehyde, 95+%;

Chemical Property of Benzaldehyde,4-(1H-pyrrol-1-yl)-

Chemical Property:

• Vapor Pressure: 0.001mmHg at 25°C
• Melting Point: 94-95 °C
• Refractive Index: 1.573
• Boiling Point: 306.656 °C at 760 mmHg
• PKA: -5.63±0.70(Predicted)
• Flash Point: 139.261 °C
• PSA: 22.00000
• Density: 1.066 g/cm³
• LogP: 2.28980
• Storage Temp.: under inert gas (nitrogen or Argon) at 2-8°C

Purity/Quality:

98%min ^*data from raw suppliers

4-(1H-Pyrrol-1-yl)benzaldehyde ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi
• Statements: 37/38-41-43
• Safety Statements: S24/25:Avoid contact with skin and eyes.

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzaldehyde,4-(1H-pyrrol-1-yl)-

There total 13 articles about Benzaldehyde,4-(1H-pyrrol-1-yl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

4-(1H-pyrrol-1-yl)-N-methoxy-N-methylbenzamide (179055-24-4) → 1-(4’-formylphenyl)pyrrole (23351-05-5)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; for 1.5h;

DOI:10.1021/jm9800853

Reference yield: 87.0%

[4-(1H-pyrrol-1-yl)phenyl]methanol (143426-51-1) → 1-(4’-formylphenyl)pyrrole (23351-05-5)

Guidance literature:

With pyridinium chlorochromate; In dichloromethane; for 1.5h; Ambient temperature;

DOI:10.1016/0223-5234(92)90005-L

Reference yield: 82.0%

→ 1-(4’-formylphenyl)pyrrole (23351-05-5)

Guidance literature:

upstream raw materials:

[4-(1H-pyrrol-1-yl)phenyl]methanol

4-(1H-pyrrol-1-yl)-N-methoxy-N-methylbenzamide

pyrrole

4-fluorobenzaldehyde

Downstream raw materials:

Cycloheptyl-(4-pyrrol-1-yl-benzyl)-amine

2,2,2-tris-methylsulfanyl-1-(4-pyrrol-1-yl-phenyl)-ethanol

(NC₅H₃CHCHC₆H₄NC₄H₄)2

1,3,4,6-tetra-O-acetyl-2-deoxy-2-[(4-(1H-pyrrol-1-yl)benzylidene)amino]-β-D-glucopyranose

Refernces

• 1、 Bhansali, Karan,Raut, Subodh,Barange, Shital,Bhagat, Pundlik. "Sulphonic acid functionalized porphyrin anchored with a: Meso -substituted triazolium ionic liquid moiety: A heterogeneous photo-catalyst for metal/base free C-C cross-coupling and C-N/C-H activation using aryl chloride under visible light irradiation". . p. 19690 - 19712. Retrieved 2020/12/04.
• 2、 -. "Two Component Recyclable Heterogeneous Catalyst, Process for Preparation Thereof and its Use for Preparation of Amines". Page/Page column 8. . Retrieved 2012/01/13.