2-(2-chlorophenyl)-4,6-dichloro-1,3,5-triazine

Base Information

• Chemical Name: 2-(2-chlorophenyl)-4,6-dichloro-1,3,5-triazine
• CAS No.: 98591-27-6
• Molecular Formula: C₉H₄Cl₃N₃
• Molecular Weight: 260.51
• Mol file: 98591-27-6.mol

Synonyms:2-(2-chlorophenyl)-4,6-dichloro-1,3,5-triazine

Chemical Property of 2-(2-chlorophenyl)-4,6-dichloro-1,3,5-triazine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-(2-chlorophenyl)-4,6-dichloro-1,3,5-triazine

There total 2 articles about 2-(2-chlorophenyl)-4,6-dichloro-1,3,5-triazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

1,3,5-trichloro-2,4,6-triazine (108-77-0) + 2-bromo-1-chlorobenzene (694-80-4) → 2-(2-chlorophenyl)-4,6-dichloro-1,3,5-triazine (98591-27-6)

Guidance literature:

2-bromo-1-chlorobenzene; With isopropylmagnesium chloride; lithium chloride; In tetrahydrofuran; at -15 - 0 ℃; for 3h; Inert atmosphere;

1,3,5-trichloro-2,4,6-triazine; In tetrahydrofuran; at 0 - 20 ℃; for 5h; Inert atmosphere;

Reference yield:

2-Chlorobenzonitrile (873-32-5) + N-Cyanoguanidine (127099-85-8,780722-26-1,461-58-5) → 2-(2-chlorophenyl)-4,6-dichloro-1,3,5-triazine (98591-27-6)

Guidance literature:

With potassium hydroxide; 2-methoxy-ethanol; und anschliessenden Erhitzen mit PCl₅ und POCl₃;

Reference yield: 58.0%

2-(2-chlorophenyl)-4,6-dichloro-1,3,5-triazine (98591-27-6) + 2-(trimethylsilyl)phenyl trifluoromethanesulfonate (88284-48-4) → 2,4,6-tris(2-chlorophenyl)-1,3,5-triazine

Guidance literature:

With potassium fluoride; 18-crown-6 ether; In tetrahydrofuran; at 0 ℃; for 15h; Inert atmosphere;

DOI:10.1246/cl.2009.1132

upstream raw materials:

2-Chlorobenzonitrile

N-Cyanoguanidine

1,3,5-trichloro-2,4,6-triazine

2-bromo-1-chlorobenzene

Refernces

• 1、 -. "METHOD FOR PRODUCING TRIARYLTRIAZINE COMPOUND". Paragraph 0145; 0146; 0147. . Retrieved 2017/11/01.