1-methylcyclobutanol acetate

Base Information

• Chemical Name: 1-methylcyclobutanol acetate
• CAS No.: 20434-37-1
• Molecular Formula: C₇H₁₂O₂
• Molecular Weight: 128.171
• Mol file: 20434-37-1.mol

Synonyms:1-methylcyclobutanol acetate

Chemical Property of 1-methylcyclobutanol acetate

Chemical Property:

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Technology Process of 1-methylcyclobutanol acetate

There total 3 articles about 1-methylcyclobutanol acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-methylcyclobutanol (20117-47-9) → decane-2,9-dione (16538-91-3) + 1-methylcyclobutanol acetate (20434-37-1) + 2-Pentanone (107-87-9)

Guidance literature:

With sodium acetate; manganese(II) acetate; In acetic acid; at 100 ℃; electrochemical oxidation;

DOI:10.1007/BF01431635

Reference yield:

1-methylcyclobutanol (20117-47-9) + manganese(II) acetate (638-38-0,993-02-2,2180-18-9,15411-95-7,22981-23-3,27004-39-3) → 4-oxopentyl acetate (5185-97-7) + decane-2,9-dione (16538-91-3) + 1-methylcyclobutanol acetate (20434-37-1) + 2-Pentanone (107-87-9)

Guidance literature:

With potassium acetate; In acetic acid; at 100 ℃; electrochemical oxidation;

DOI:10.1007/BF01431635

Reference yield:

1-methylcyclobutanol (20117-47-9) + manganese(II) acetate (638-38-0,993-02-2,2180-18-9,15411-95-7,22981-23-3,27004-39-3) → 5-chloro-2-pentanone (5891-21-4) + 1-methylcyclobutanol acetate (20434-37-1) + 2-Pentanone (107-87-9)

Guidance literature:

With sodium acetate; lithium chloride; In acetic acid; at 50 ℃; Product distribution; other reaction products at different reagents and conditions of electrolysis;

DOI:10.1007/BF01431635

upstream raw materials:

1-methylcyclobutanol

manganese(II) acetate

Refernces