Technology Process of <(Z)-4-Nonenyl>-triphenylphosphonium-bromid
There total 10 articles about <(Z)-4-Nonenyl>-triphenylphosphonium-bromid which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 75 percent / nickel acetate, sodium borohydride, ethylenediamine, hydrogen / ethanol
2: 65 percent / pyridine, phosphorus tribromide / benzene / 6 h / Heating
3: tetrahydrofuran / Ambient temperature
With
pyridine; sodium tetrahydroborate; hydrogen; nickel diacetate; phosphorus tribromide; ethylenediamine;
In
tetrahydrofuran; ethanol; benzene;
- Guidance literature:
-
Multi-step reaction with 5 steps
2: 81 percent / LiNH2, NH3 (liquid) / 4 h
3: H2, Na/NH3 / Ni(OAc)2.4H2O, NaBH4
4: 78 percent / triphenylphosphine, Br2, pyridine / CH2Cl2; CCl4 / 2 h / Ambient temperature
5: 23.4 g / acetonitrile / 24 h / Heating
With
pyridine; lithium amide; ammonia; hydrogen; bromine; sodium; triphenylphosphine;
sodium tetrahydroborate; nickel diacetate;
In
tetrachloromethane; dichloromethane; acetonitrile;
DOI:10.1016/0040-4020(84)85012-7
